trichlorophosphate in acetonitrile
1.5 h; Heating;
参考文献
Gibson, Scott L.; Holt, Jason J.; Ye, Mao; Donnelly, David J.; Ohulchanskyy, Tymish Y.; You, Youngjae; Detty, Michael R.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 23 p. 6394 - 6403
1.1: Mg / tetrahydrofuran / 2 h / Heating
1.2: sulfur / tetrahydrofuran / 2 h / Heating
2.1: 0.79 g / dihexyl telluride; H2O2 / 1 h
3.1: sec-butyllithium; N,N,N',N'-tetramethylethylenediamine / tetrahydrofuran; cyclohexane / 1 h / -78 °C
3.2: 51 percent / tetrahydrofuran; cyclohexane / -78 - 20 °C
4.1: 13 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 15 h / 25 °C
View Scheme
参考文献
Detty, Michael R.; Prasad, Paras N.; Donnelly, David J.; Ohulchanskyy, Tymish; Gibson, Scott L.; Hilf, Russell
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 10 p. 2537 - 2544
1.1: 0.79 g / dihexyl telluride; H2O2 / 1 h
2.1: sec-butyllithium; N,N,N',N'-tetramethylethylenediamine / tetrahydrofuran; cyclohexane / 1 h / -78 °C
2.2: 51 percent / tetrahydrofuran; cyclohexane / -78 - 20 °C
3.1: 13 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 15 h / 25 °C
View Scheme
参考文献
Detty, Michael R.; Prasad, Paras N.; Donnelly, David J.; Ohulchanskyy, Tymish; Gibson, Scott L.; Hilf, Russell
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 10 p. 2537 - 2544
1.1: sec-butyllithium; N,N,N',N'-tetramethylethylenediamine / tetrahydrofuran; cyclohexane / 1 h / -78 °C
1.2: 51 percent / tetrahydrofuran; cyclohexane / -78 - 20 °C
2.1: 13 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 15 h / 25 °C
View Scheme
参考文献
Detty, Michael R.; Prasad, Paras N.; Donnelly, David J.; Ohulchanskyy, Tymish; Gibson, Scott L.; Hilf, Russell
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 10 p. 2537 - 2544
