1,3-苯并间二氧杂环戊烯-5-丙醇合成路线 （共 29 条）
参考文献
Texas Biotechnology Corporation
Patent: US5804585 A1, 1998 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
3 h;
参考文献
Schobert; Siegfried; Gordon
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 19 p. 2393 - 2397
反应条件
copper oxide-chromium oxide
T=255°C; P=95616 Torr; Hydrogenation;
参考文献
Kondo et al.
Itsuu Kenkyusho Nempo, 1951 , # 2 p. 24,27; engl. Ref. S. 60, 64
Chem.Abstr., 1953 , p. 7516
参考文献
Bogert; Powell
Journal of the American Chemical Society, 1931 , vol. 53, p. 2747,2752
反应条件
sodium; toluene; butan-1-ol
参考文献
Orcutt; Bogert
Journal of the American Chemical Society, 1936 , vol. 58, p. 2055
反应条件
1: benzene / 4 h / Heating
2: LiAlH4; AlCl3 / tetrahydrofuran / 1 h / 0 °C
3: H2 / Pd/C
View Scheme
参考文献
Li, Yang; Zhang, Yu; Huang, Zhi; Cao, Xiaoping; Gao, Kun
Canadian Journal of Chemistry, 2004 , vol. 82, # 5 p. 622 - 630
反应条件
1: LiAlH4; AlCl3 / tetrahydrofuran / 1 h / 0 °C
2: H2 / Pd/C
View Scheme
参考文献
Li, Yang; Zhang, Yu; Huang, Zhi; Cao, Xiaoping; Gao, Kun
Canadian Journal of Chemistry, 2004 , vol. 82, # 5 p. 622 - 630
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
32 h;
参考文献
Bailey, Patrick D.; Morgan, Keith M.; Smith, David I.; Vernon, John M.
Tetrahedron, 2003 , vol. 59, # 18 p. 3369 - 3378
反应条件
hydrogen; palladium on activated charcoal
参考文献
Li, Yang; Zhang, Yu; Huang, Zhi; Cao, Xiaoping; Gao, Kun
Canadian Journal of Chemistry, 2004 , vol. 82, # 5 p. 622 - 630
反应条件
NaBO3; borane
1.) THF, from 0 deg C to RT, 2 h, 2.) H2O, 25 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kabalka, George W.; Shoup, Timothy M.; Goudgaon, Naganna M.
Journal of Organic Chemistry, 1989 , vol. 54, # 25 p. 5930 - 5933
