3-苯甲酰噻唑烷-2-硫酮合成路线 （共 21 条）
反应条件
triethylamine in dichloromethane
T=20°C; Cooling with ice;
参考文献
Shanghai Institute of Materia Medica, Chinese Academy of Sciences
Patent: EP2119720 A1, 2009 ;
Location in patent: Page/Page column 21 ;
反应条件
DMEG; triethylamine in dichloromethane
T=20°C; Acylation; 48 h;
参考文献
Isobe, Toshio; Ishikawa, Tsutomu
Journal of Organic Chemistry, 1999 , vol. 64, # 19 p. 6984 - 6988
反应条件
dicyclohexyl-carbodiimide in ethyl acetate
24 h; Ambient temperature;
参考文献
Nagao, Yoshimitsu; Kawabata, Kohji; Seno, Kaoru; Fujita, Eiichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2470 - 2473
反应条件
in tetrahydrofuran
3 h; Ambient temperature;
参考文献
Nagao, Yoshimitsu; Kawabata, Kohji; Seno, Kaoru; Fujita, Eiichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2470 - 2473
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=0°C;
参考文献
Yamada, M.; Yahiro, S.; Yamano, T.; Nakatani, Y.; Ourisson, G.
Bulletin de la Societe Chimique de France, 1990 , # 6 p. 824 - 829
反应条件
in dichloromethane
0.666667 h; Ambient temperature;
参考文献
Nagao, Yoshimitsu; Seno, Kaoru; Kawabata, Kohji; Miyasaka, Tadao; Takao, Sachiko; Fujita, Eiichi
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 7 p. 2687 - 2699
反应条件
in dichloromethane
0.0833333 h; Ambient temperature;
参考文献
Nagao, Yoshimitsu; Seno, Kaoru; Kawabata, Kohji; Miyasaka, Tadao; Takao, Sachiko; Fujita, Eiichi
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 7 p. 2687 - 2699
反应条件
in dichloromethane
3 h; Ambient temperature;
参考文献
Nagao, Yoshimitsu; Seno, Kaoru; Kawabata, Kohji; Miyasaka, Tadao; Takao, Sachiko; Fujita, Eiichi
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 7 p. 2687 - 2699
反应条件
cesium fluoride in N,N-dimethyl-formamide
T=80°C; 5 h;
参考文献
Yamada, M.; Yahiro, S.; Yamano, T.; Nakatani, Y.; Ourisson, G.
Bulletin de la Societe Chimique de France, 1990 , # 6 p. 824 - 829
参考文献
Nagao, Yoshimitsu; Yagi, Masahiro; Ikede, Takao; Fujita, Eiichi
Tetrahedron Letters, 1982 , vol. 23, # 2 p. 201 - 204
