4,6-二甲基-5-羟基嘧啶合成路线 (共 5 条)
反应条件
para-nitroperbenzoic acid in acetone
T=25 - 40°C;
参考文献
Gashev, S. B.; Lezina, V. P.; Smirnov, L. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1003 - 1007
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1252 - 1256
反应条件
1: 96 percent / p-nitroperbenzoic acid / acetone / 25 - 40 °C
2: 63 percent / dioxane / 0.03 h / 70 °C
View Scheme
参考文献
Gashev, S. B.; Lezina, V. P.; Smirnov, L. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1003 - 1007
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1252 - 1256
反应条件
1: 96 percent / p-nitroperbenzoic acid / acetone / 25 - 40 °C
2: 66 percent / 0.25 h / Heating
View Scheme
参考文献
Gashev, S. B.; Lezina, V. P.; Smirnov, L. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1003 - 1007
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1252 - 1256
反应条件
1: 96 percent / p-nitroperbenzoic acid / acetone / 25 - 40 °C
2: 85 percent / benzene / 0.17 h / Heating
View Scheme
参考文献
Gashev, S. B.; Lezina, V. P.; Smirnov, L. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1003 - 1007
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1252 - 1256
反应条件
1: 96 percent / p-nitroperbenzoic acid / acetone / 25 - 40 °C
2: 5 percent / H2O / 3 h / 70 °C
View Scheme
参考文献
Gashev, S. B.; Lezina, V. P.; Smirnov, L. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1003 - 1007
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1252 - 1256