1: Li / diethyl ether / 25 °C
2: diethyl ether / 25 °C
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参考文献
Hitchcock, Peter B.; Lappert, Michael F.; Power, Philip P.; Smith, Stephen J.
Journal of the Chemical Society, Chemical Communications, 1984 , # 24 p. 1669 - 1670
Hitchcock, Peter B.; Lappert, Michael F.; Power, Philip P.; Smith, Stephen J.
Journal of the Chemical Society, Chemical Communications, 1984 , # 24 p. 1669 - 1670
in benzene-d6
dissolved in benzene under inert atm.; free phosphine is present in 12percent to total phosphorus content at 21°C, shift of the equil. upon addn. of 1 equiv of phosphine ligand or (RhCl(COD))2 confirmes the reversibility of the reaction; (31)P and (1)H NMR spectral data;
参考文献
Murray, Brendan D.; Hope, Hakon; Hvoslef, Jan; Power, Philip P.
Organometallics, 1984 , vol. 3, p. 657 - 663
