potassium dihydrogenphosphate; Fremy’s salt in water; acetone
0.5 h; Ambient temperature;
参考文献
Martin, Tracey; Moody, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 235 - 240
1: 98 percent / H2SO4
2: 69 percent / NaOMe / dioxane / 45 h / 110 °C
3: 94 percent / water / aq. NaOH / dioxane / 17 h / 110 °C
4: 70 percent / PCC / CH2Cl2 / 2 h / Ambient temperature
5: 59 percent / BF3*MeOH / 17 h / Ambient temperature; reaction of its derivatives HCl too with sev. alcohols
6: 86 percent / BBr3 / CH2Cl2 / 16 h / -78 °C
7: 85 percent / Fremy's salt, KH2PO4 / H2O; acetone / 0.5 h / Ambient temperature
View Scheme
参考文献
Martin, Tracey; Moody, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 235 - 240
1: 69 percent / NaOMe / dioxane / 45 h / 110 °C
2: 94 percent / water / aq. NaOH / dioxane / 17 h / 110 °C
3: 70 percent / PCC / CH2Cl2 / 2 h / Ambient temperature
4: 59 percent / BF3*MeOH / 17 h / Ambient temperature; reaction of its derivatives HCl too with sev. alcohols
5: 86 percent / BBr3 / CH2Cl2 / 16 h / -78 °C
6: 85 percent / Fremy's salt, KH2PO4 / H2O; acetone / 0.5 h / Ambient temperature
View Scheme
参考文献
Martin, Tracey; Moody, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 235 - 240
1: 86 percent / BBr3 / CH2Cl2 / 16 h / -78 °C
2: 85 percent / Fremy's salt, KH2PO4 / H2O; acetone / 0.5 h / Ambient temperature
View Scheme
参考文献
Martin, Tracey; Moody, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 235 - 240
Bernardo, Paul H.; Chai, Christina L.L.; Guen, Maurice Le; Smith, Geoffrey D.; Waring, Paul
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 1 p. 82 - 85