[(3-丁烯-1-基氧基)甲基]苯合成路线 （共 32 条）
反应条件
1: titanium(IV) isopropylate With n-butyllithium in tetrahydrofuran T=0°C; 0.0833333 h; Inert atmosphere; 2: ((but-3-en-1-yloxy)methyl)benzene in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 3: carbon dioxide in tetrahydrofuran T=0°C; 0.333333 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 70, # 4 p. 787 - 794
反应条件
Mo(CHCMe2Ph)(NAr)lt;OCMe(CF3)2gt;2 (Schrock's molybdenum catalyst) in ethylene glycol dimethyl ether 4 h; Yields of byproduct given;
参考文献
Crowe, William E.; Goldberg, Daniel R.; Zhang, Zhijia J.
Tetrahedron Letters, 1996 , vol. 37, # 13 p. 2117 - 2120
反应条件
1.1: O3 / CH2Cl2 / -78 °C 1.2: 86 percent / Ph3P 2.1: CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Hon, Yung-Son; Lu, Ling; Chang, Rong-Chi; Lin, Sheng-Wun; Sun, Pei-Pei; Lee, Chia-Fu
Tetrahedron, 2000 , vol. 56, # 47 p. 9269 - 9279
反应条件
1: With ozone in dichloromethane T=-78°C; 2: With triphenylphosphine
参考文献
Hon, Yung-Son; Lu, Ling; Chang, Rong-Chi; Lin, Sheng-Wun; Sun, Pei-Pei; Lee, Chia-Fu
Tetrahedron, 2000 , vol. 56, # 47 p. 9269 - 9279
反应条件
oxygen; 1-n-butyl-3-methylimidazolium tetrafluoroborate; copper(l) chloride; palladium dichloride in water T=60°C; Wacker oxidation; 25 h;
参考文献
Ansari; Joyasawal, Sipak; Gupta, Manoj K.; Yadav; Gree
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7507 - 7510
反应条件
sodium hydroxide; triethylamine in hexane
3 h; Heating;
参考文献
Xu, Yao-Chang; Kohlman, Dan T.; Liang, Sidney X.; Erikkson, Chad
Organic Letters, 1999 , vol. 1, # 10 p. 1599 - 1602
反应条件
1: With IPNBSH; triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
T=0 - 23°C; Mitsunobu reaction; 2 h;
2: in 2,2,2-trifluoroethanol; water
T=23°C; 3 h;
参考文献
Movassaghi, Mohammad; Ahmad, Omar K.
Journal of Organic Chemistry, 2007 , vol. 72, # 5 p. 1838 - 1841
反应条件
potassium hydroxide
T=80°C; 72 h;
参考文献
Murphy, Stephen K.; Petrone, David A.; Coulter, Matthew M.; Dong, Vy M.
Organic Letters, 2011 , vol. 13, # 23 p. 6216 - 6219
反应条件
potassium tert-butylate; Aliquatreg; 336
T=25°C; 4 h;
参考文献
Berranger; Langlois
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1720 - 1726
反应条件
hydrogen; N1-(2-Amino-ethyl)-ethane-1,2-diamine in methanol
T=25°C; 6 h;
参考文献
Yabe, Yuki; Yamada, Tsuyoshi; Nagata, Saori; Sawama, Yoshinari; Monguchi, Yasunari; Sajiki, Hironao
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 7 p. 1264 - 1268
