2-甲氧基-4-甲基苯甲酸合成路线 (共 33 条)
参考文献
Bulletin de la Societe Chimique de France, , p. 2255 - 2261
反应条件
N,N,N',N'',N''-pentamethyldiethylenetriamine; tert.-butyl lithium 1.) hexane, 25 deg C, 16 h.; Multistep reaction;
参考文献
Tetrahedron, , vol. 54, # 12 p. 2763 - 2770
反应条件
1: aq. NaOH 2: aq. NaOCl View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 2255 - 2261
反应条件
1: AlCl3 / 165 °C 2: aq. NaOH 3: aq. NaOCl View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 2255 - 2261
参考文献
Journal of the Chemical Society, , vol. 89, p. 1655
反应条件
(i) O3, AcOEt, (ii) H2O, (iii) aq. H2O2, aq. NaOH; Multistep reaction;
参考文献
Chemical and pharmaceutical bulletin, , vol. 13, # 1 p. 64 - 69
参考文献
Zhurnal Obshchei Khimii, , vol. 2, p. 472,475
Chem. Zentralbl., , vol. 104, # I p. 604
参考文献
Chem. Zentralbl., , vol. 75, # I p. 1597
参考文献
Justus Liebigs Annalen der Chemie, , vol. 442, p. 41
反应条件
1.1: thionyl chloride / 3 h / |Inert atmosphere; |Reflux 2.1: dichloromethane / 12 h / 0 - 20 °C / |Inert atmosphere 3.1: sec.-butyllithium; N,N,N',N,-tetramethylethylenediamine / tetrahydrofuran; cyclohexane / 2 h / -78 °C / |Inert atmosphere 3.2: -78 - 20 °C / |Inert atmosphere 4.1: hydrogenchloride; acetic acid; water / 12 h / |Reflux View Scheme
参考文献
Mamidyala, Sreeman K.; Cooper, Matthew A.
Chemical Communications, 2013 , vol. 49, # 75 p. 8407 - 8409