hydrogenchloride; hydrogen; palladium on activated charcoal in N,N-dimethyl-formamide
4 h;
参考文献
Nanayakkara, N. P. Dhammika; Hussain, Raouf A.; Pezzuto, John M.; Soejarto, D. Doel; Kinghorn, A. Douglas
Journal of Medicinal Chemistry, 1988 , vol. 31, # 6 p. 1250 - 1253
1: 82 percent / K2CO3 / dimethylformamide / 5 h / 120 °C
2: 89.3 percent / 7.1 N NaOH, 30percent H2O2 / CHCl3; methanol / 18 h / Ambient temperature
3: 88 percent / HCl, H2 / Pd/C / dimethylformamide / 4 h
View Scheme
参考文献
Nanayakkara, N. P. Dhammika; Hussain, Raouf A.; Pezzuto, John M.; Soejarto, D. Doel; Kinghorn, A. Douglas
Journal of Medicinal Chemistry, 1988 , vol. 31, # 6 p. 1250 - 1253
1: 89.3 percent / 7.1 N NaOH, 30percent H2O2 / CHCl3; methanol / 18 h / Ambient temperature
2: 88 percent / HCl, H2 / Pd/C / dimethylformamide / 4 h
View Scheme
参考文献
Nanayakkara, N. P. Dhammika; Hussain, Raouf A.; Pezzuto, John M.; Soejarto, D. Doel; Kinghorn, A. Douglas
Journal of Medicinal Chemistry, 1988 , vol. 31, # 6 p. 1250 - 1253
