(S)-2-甲基-1,4-丁二醇合成路线 （共 57 条）
反应条件
1: sodium periodate; ruthenium(III) chloride*(x)H2O / tetrachloromethane; acetonitrile; water / 1 h / 20 °C 2: borane-THF / tetrahydrofuran / 3.5 h / 20 °C 3: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 2 p. 614 - 627
反应条件
1: borane-THF / tetrahydrofuran / 3.5 h / 20 °C 2: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 2 p. 614 - 627
反应条件
1: n-butyllithium; borane-ammonia complex; diisopropylamine / tetrahydrofuran / 2 h / 0 °C 2: 1H-imidazole; 4-(N,N-dimethlyamino)pyridine / tetrahydrofuran / 18 h / 20 °C 3: sodium periodate; ruthenium(III) chloride*(x)H2O / tetrachloromethane; acetonitrile; water / 1 h / 20 °C 4: borane-THF / tetrahydrofuran / 3.5 h / 20 °C 5: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 2 p. 614 - 627
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 1 h; enantioselectivity;
参考文献
Synthetic Communications, , vol. 17, # 3 p. 241 - 250
反应条件
lithium aluminium tetrahydride
参考文献
Bulletin des Societes Chimiques Belges, , vol. 101, # 7 p. 627 - 640
反应条件
lithium aluminium tetrahydride; Raney Nickel (RaNi) Multistep reaction;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 101, # 7 p. 627 - 640
反应条件
in chloroform T=30°C; 4 h; Pseudomonas fluorescens lipase (PFL); var. times, also benzyl ether derivatives; Product distribution;
参考文献
Grisenti; Ferraboschi; Casati; Santaniello
Tetrahedron Asymmetry, 1993 , vol. 4, # 5 p. 997 - 1006
