2,3,3',4,5-五氯联苯合成路线 （共 9 条）
反应条件
in cyclohexane
19 h; Irradiation;
参考文献
Pyle, James L.; Shaffer, Alan A.; Cantrell, Joseph S.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 115 - 118
反应条件
1: KOH / aq. ethanol / 12 h / Heating
2: 80.6 percent / benzene
3: 44.7 percent / cyclohexane / 19 h / Irradiation
View Scheme
参考文献
Pyle, James L.; Shaffer, Alan A.; Cantrell, Joseph S.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 115 - 118
反应条件
1: 1.25 h / 63 - 75 °C
2: KOH / aq. ethanol / 12 h / Heating
3: 80.6 percent / benzene
4: 44.7 percent / cyclohexane / 19 h / Irradiation
View Scheme
参考文献
Pyle, James L.; Shaffer, Alan A.; Cantrell, Joseph S.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 115 - 118
反应条件
1: hydroquinone, PCl5
2: 1.25 h / 63 - 75 °C
3: KOH / aq. ethanol / 12 h / Heating
4: 80.6 percent / benzene
5: 44.7 percent / cyclohexane / 19 h / Irradiation
View Scheme
参考文献
Pyle, James L.; Shaffer, Alan A.; Cantrell, Joseph S.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 115 - 118
反应条件
copper in N,N-dimethyl-formamide
Ulman reaction; Heating;
参考文献
Bolgar; et al.
Chemosphere, 1995 , vol. 31, # 2 p. 2687 - 2705
反应条件
1: 80.6 percent / benzene
2: 44.7 percent / cyclohexane / 19 h / Irradiation
View Scheme
参考文献
Pyle, James L.; Shaffer, Alan A.; Cantrell, Joseph S.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 115 - 118
反应条件
oxygen
T=550 - 600°C; 0.00138889 h; Product distribution;
参考文献
Mazer, Thomas; Hileman, Fred D.; Noble, Roy W.; Brooks, Joseph J.
Analytical Chemistry, 1983 , vol. 55, # 1 p. 104 - 110
反应条件
oxygen
T=550 - 600°C; 0.00138889 h; Product distribution;
参考文献
Mazer, Thomas; Hileman, Fred D.; Noble, Roy W.; Brooks, Joseph J.
Analytical Chemistry, 1983 , vol. 55, # 1 p. 104 - 110
反应条件
oxygen
T=550 - 600°C; 0.00138889 h; Product distribution;
参考文献
Mazer, Thomas; Hileman, Fred D.; Noble, Roy W.; Brooks, Joseph J.
Analytical Chemistry, 1983 , vol. 55, # 1 p. 104 - 110
