2,3,5,6-四氯-4-甲氧基苯胺合成路线 （共 7 条）
反应条件
N-chloro-succinimide in toluene
T=80°C; 1 h;
参考文献
Hovander; Malmberg; Athanasiadou; Athanassiadis; Rahm; Bergman; Wehler, E. Klasson
Archives of Environmental Contamination and Toxicology, 2002 , vol. 42, # 1 p. 105 - 117
反应条件
1: 90 percent / SnCl2*2H2O / ethanol; HCl / 1 h / 60 °C
2: 90 percent / NCS / toluene / 1 h / 80 °C
View Scheme
参考文献
Hovander; Malmberg; Athanasiadou; Athanassiadis; Rahm; Bergman; Wehler, E. Klasson
Archives of Environmental Contamination and Toxicology, 2002 , vol. 42, # 1 p. 105 - 117
反应条件
sodium hydroxide; ethanol
参考文献
Bures; Hutter
C.csl.Lekarn., 1931 , vol. 11, p. 57,58
Chem. Zentralbl., 1931 , vol. 102, # II p. 225
反应条件
1: HNO3 / 0 °C
2: sodium dithionite; aqueous ethanol
View Scheme
参考文献
Peters; Rowe; Stead
Journal of the Chemical Society, 1943 , p. 233
反应条件
1: Fe, aq. NH4Cl
View Scheme
参考文献
Kobrina,L.S.; Yakobson,G.G.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, # 11 p. 2055 - 2062,2046 - 2052
参考文献
Kobrina,L.S.; Yakobson,G.G.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, # 11 p. 2055 - 2062,2046 - 2052
反应条件
sulfuric acid; sodium sulfate
T=150°C; Diazotization;
参考文献
Bures; Hutter
C. csl. Lekarn., 1931 , vol. 11, p. 57,60
