1.1: 83 percent / aq. ceric ammonium nitrate / acetonitrile / 1 h / 0 °C 2.1: aq. LiOH / tetrahydrofuran / 96 h / 5 °C 3.1: bis(2-oxo-3-oxazolidinyl)phosphonic chloride; pyridine / CH2Cl2 / 1 h / 23 °C 3.2: 100 mg / pyridine; PPh3Cl2 / acetonitrile; CH2Cl2 / 1 h / 23 °C View Scheme