4-乙炔基-α,α,α-三氟甲苯合成路线 (共 50 条)
反应条件
1: 60 percent / P2O5 / benzene / 4 h / Heating 2: Br2 / diethyl ether / 2 h / -10 °C 3: 50 percent / KOH / H2O; diethyl ether / 180 - 220 °C View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 9 p. 3216 - 3245
参考文献
Journal of the American Chemical Society, , vol. 85, p. 3492 - 3496
反应条件
2: KHSO4 3: (i) Br2, (ii) KOH 4: KOH View Scheme
参考文献
Journal of the American Chemical Society, , vol. 85, p. 3492 - 3496
反应条件
manganese(IV) oxide; potassium hydroxide in diethyl ether T=20°C; 2 h;
参考文献
Chemistry - A European Journal, , vol. 14, # 12 p. 3670 - 3679
反应条件
1: palladium on copper / |Inert atmosphere 2: potassium carbonate; methanol / |Inert atmosphere View Scheme
参考文献
Chemistry Letters, , vol. 42, # 10 p. 1128 - 1130
反应条件
1: 43 percent / p-TsOH / benzene / 6 h / Heating 2: pentane / 23 °C / Irradiation; also in acetonitrile View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 73, # 2 p. 191 - 203
反应条件
1: chloroform / 20 - 60 °C / Irradiation; Bromination 2: potassium carbonate / dimethyl sulfoxide / 12 h / 115 °C View Scheme
参考文献
Chinese Journal of Chemistry, , vol. 29, # 11 p. 2350 - 2354
反应条件
1: 1.) n-C4H9Li 2: n-C4H9Li View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 23, p. 497
反应条件
in pentane T=23°C; Irradiation;
参考文献
Canadian Journal of Chemistry, , vol. 73, # 2 p. 191 - 203
反应条件
T=23°C; Irradiation; Quantum yieldRate constant;
参考文献
Canadian Journal of Chemistry, , vol. 73, # 2 p. 191 - 203