N,N-二甲基-6-丙酰-2-萘胺合成路线 （共 2 条）
反应条件
1: 2-bromo-6-(N,N-dimethylamino)naphthalene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: 1-(1H-pyrrol-1-yl)propan-1-one in tetrahydrofuran; hexane T=-45°C; 1.5 h;
参考文献
Silvonek, Steven S.; Giller, Carl B.; Abelt, Christopher J.
Organic Preparations and Procedures International, 2005 , vol. 37, # 6 p. 589 - 594
反应条件
1.1: 80 percent / K2CO3 / dimethylformamide / 20 °C 2.1: 82 percent / ethanolamine / 1 h / 150 °C 3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C 3.2: 580 mg / tetrahydrofuran; hexane / 1.5 h / -45 °C View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 37, # 6 p. 589 - 594
