反应条件
1: 3-(5-methyl-2-furanyl)-1-propanol With sulfur trioxide pyridine complex; triethylamine in dimethyl sulfoxide
T=0°C; 1 h;
2: carbon tetrabromide With triethylamine; triphenylphosphine in dichloromethane
T=-20 - 20°C;
3: With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.166667 h; Further stages.;
参考文献
Yamamoto, Hirofumi; Sasaki, Ikuo; Imagawa, Hiroshi; Nishizawa, Mugio
Organic Letters, 2007 , vol. 9, # 7 p. 1399 - 1402