(Z)-3-(吡咯烷-1-基)2-丁酸乙酯合成路线 （共 16 条）
反应条件
[PtCl2(η2:η2-cycloocta-1,5-diene)]; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=60°C; 5 h; Inert atmosphereSchlenk techniqueMicrowave irradiation; regioselective reaction;
参考文献
Shibuya, Ryozo; Lin, Lu; Nakahara, Yasuhito; Mashima, Kazushi; Ohshima, Takashi
Angewandte Chemie - International Edition, 2014 , vol. 53, # 17 p. 4377 - 4381
Angew. Chem., 2014 , vol. 126, # 17 p. 4466 - 4470,5
反应条件
[((1,2-bis(diphenylphosphino)ethane))Ni]-(OTf)2 in tetrahydrofuran T=100°C; 4 h; Schlenk techniqueInert atmosphere; Reagent/catalyst;
参考文献
Reyes-Sanchez, Adan; Garcia-Ventura, Ilnett; Garcia, Juventino J.
Dalton Transactions, 2014 , vol. 43, # 4 p. 1762 - 1768
反应条件
triethylamine; trichlorophosphate in chloroform
参考文献
Hoffmann-La Roche Inc.
Patent: US3984427 A1, 1976 ;
反应条件
potassium acetate in ethanol T=25°C; 1.41667 h;
参考文献
Alberola, A.; Calvo, L. A.; Ortega, A. Gonzalez; Sadaba, M. L.; Sanudo, M. C.
Anales de Quimica, 1995 , vol. 91, # 3-4 p. 284 - 289
反应条件
hydrogenchloride in ethanol T=25°C; 2.91667 h;
参考文献
Alberola, A.; Calvo, L. A.; Ortega, A. Gonzalez; Sadaba, M. L.; Sanudo, M. C.
Anales de Quimica, 1995 , vol. 91, # 3-4 p. 284 - 289
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); triethylamine in acetonitrile T=-10°C; 0.5 h;
参考文献
Peng, Weimin; Shreeve, Jean'ne M.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5760 - 5763
反应条件
in diethyl ether 72 h; Heating1.) ether, reflux, 3 days; 2.) water, 30 deg C, 15 min;
参考文献
Baron, Michel; Cointet, Paul de; Bauduin, Gerard; Pietrasanta, Yves; Pucci, Bernard
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 7/8 p. 249 - 256
反应条件
sodium; isopropyl alcohol in tetrahydrofuran T=0°C;
参考文献
Bartoli; Cimarelli; Marcantoni; Palmieri; Petrini
Journal of Organic Chemistry, 1994 , vol. 59, # 18 p. 5328 - 5335
反应条件
in dichloromethane T=20°C; 0.5 h;
参考文献
Zhu, Shizheng; Jin, Guifang; Xu, Yong
Tetrahedron, 2003 , vol. 59, # 24 p. 4389 - 4394
反应条件
in dichloromethane T=20°C; 0.5 h;
参考文献
Zhu, Shizheng; Jin, Guifang; Xu, Yong
Tetrahedron, 2003 , vol. 59, # 24 p. 4389 - 4394
