2-碘甲基-4,4,5,5-四甲基-1,3,2-二氧硼戊环合成路线 （共 16 条）
反应条件
sodium iodide; methyl iodide in N,N-dimethyl-formamide
参考文献
Matteson,D.S.; Majumdar,D.
Journal of Organometallic Chemistry, 1979 , vol. 170, p. 259 - 264
反应条件
1: 3 h / 115 °C
2: n-BuLi / tetrahydrofuran / 20 °C
View Scheme
参考文献
Smoum, Reem; Rubinstein, Abraham; Srebnik, Morris
Bioorganic Chemistry, 2003 , vol. 31, # 6 p. 464 - 474
参考文献
Molander, Gary A.; Febo-Ayala, Wilma; Ortega-Guerra, Montserrat
Journal of Organic Chemistry, 2008 , vol. 73, # 15 p. 6000 - 6002
反应条件
in acetone
(Ar); refluxed for 48 h; volatiles distd., fractionally distd.; elem. anal.;
参考文献
Wuts, Peter G. M.; Thompson, Paul A.
Journal of Organometallic Chemistry, 1982 , vol. 234, # 2 p. 137 - 142
参考文献
Reddy, Venkata Jaganmohan; Chandra, J. Subash; Reddy, M. Venkat Ram
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 6 p. 889 - 891
反应条件
potassium in benzene
soln. (pinacolato)BCH2I in benzene was added slowly to mixt. K and benzene and heated under reflux overnight; solids were filtered, solvent was removed under vac., products were purified by chromy. on silica (10 percent Et2O/petroleum ether); elem. anal.;
参考文献
Ali, Hijazi Abu; Goldberg, Israel; Srebnik, Morris
Organometallics, 2001 , vol. 20, # 18 p. 3962 - 3965
