反应条件
1.1: sec-butyllithium; N,N,N',N'-tetramethylethylenediamine / tetrahydrofuran; cyclohexane / 1 h / -78 °C
1.2: 51 percent / tetrahydrofuran; cyclohexane / -78 - 20 °C
2.1: 13 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 15 h / 25 °C
View Scheme
参考文献
Detty, Michael R.; Prasad, Paras N.; Donnelly, David J.; Ohulchanskyy, Tymish; Gibson, Scott L.; Hilf, Russell
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 10 p. 2537 - 2544
