反-4-氯-β-硝基苯乙烯合成路线 （共 30 条）
反应条件
in acetonitrile T=30°C; var. temp.; Equilibrium constant;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, , vol. 30, # 7 p. 609 - 613
反应条件
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.33 h / 0 - 45 °C / Inert atmosphere 2.1: sodium carbonate / chloroform / 3 h / 20 °C 3.1: trichlorophosphate; phosphorous pentoxide / 3 h / Reflux 3.2: 20 °C View Scheme
参考文献
NOVARTIS AG; Bock, Mark Gary; Gaul, Christoph; Gummadi, Venkateshwar Rao; Moebitz, Henrik; Sengupta, Saumitra
Patent: US2014/45872 A1, 2014 ;
反应条件
1,5,7-triazabicyclo [4.4.0] dec-5-ene immobilized on SBA-15 T=-0.16°C; Michael addition; 9 h; Inert atmosphere;
参考文献
Kalita, Pranjal; Kumar, Rajiv
Applied Catalysis A: General, 2011 , vol. 397, # 1-2 p. 250 - 258
反应条件
1: 4-(N,N-dimethlyamino)pyridine / acetonitrile / 30 °C 2: pyridine / dichloromethane / 0.5 h / 0 °C 3: methanol / 0.33 h / 30 °C 4: water; potassium hydroxide / ethanol / 30 °C View Scheme
参考文献
Nair, Divya K.; Mobin, Shaikh M.; Namboothiri, Irishi N.N.
Organic Letters, 2012 , vol. 14, # 17 p. 4580 - 4583
反应条件
1.1: Takamoto's catalist / toluene / 24 h / 20 °C / Inert atmosphere 2.1: hydrogen / nickel / isopropyl alcohol; toluene / 71 °C / 3750.38 Torr / Inert atmosphere 3.1: hydrogenchloride; water / 1,2-dichloro-benzene / 24 h / 100 °C 3.2: 70 - 111 °C 4.1: sodium hydroxide / water / 25 °C / pH 7.3 / Activated carbon View Scheme
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: US2011/152572 A1, 2011 ;
反应条件
piperidine in diethyl ether
参考文献
Hassner, Alfred; Dehaen, Wim
Journal of Organic Chemistry, 1990 , vol. 55, # 20 p. 5505 - 5510
反应条件
C23H37N3O9S in toluene T=-20°C; asymmetric Michael addition; 20 h; enantioselective reaction;
参考文献
Li, Xiao-Juan; Liu, Kun; Ma, Hai; Nie, Jing; Ma, Jun-An
Synlett, 2008 , # 20 p. 3242 - 3246
反应条件
in ethanol 3 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 21, # 9 p. 872 - 874
反应条件
titanium tetrachloride; tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide electroreduction - 4 mA/cm2;
参考文献
Sera, Akira; Tani, Hiroyuki; Nishiguchi, Ikuzo; Hirashima, Tsuneaki
Synthesis, 1987 , # 7 p. 631 - 633
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
European Journal of Medicinal Chemistry, , vol. 18, # 4 p. 319 - 329
