反,反,顺-1,5,9-环十二烷基三烯合成路线 (共 58 条)
反应条件
diethylaluminium chloride; titanium tetrachloride in benzene T=60°C; 8 h; <6+2> cycloadditions with dienes and acetylenes catalyzed by titanium complexes, investigation of the complex of CHT with Ti(II)(AlCl4)2 and (η6-C6H6)Ti(II)(AlCl4)2;
参考文献
Tetrahedron, , vol. 40, # 17 p. 3295 - 3302
反应条件
triethylaluminum; 2,2'-dipyridylmethane-Ni(OAc)2 in toluene T=80°C; 64 h; variation of catalyst, reaction temperature and time; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 335, p. 125 - 132
反应条件
byproducts: phenol; P(OC6H5)3 in excess; at room temp.; distn. in high vac.;
反应条件
copper 1.) ether 2.) 180 deg C, 20 Torr then 1 Torr;
参考文献
Tetrahedron, , vol. 42, # 6 p. 1711 - 1720
反应条件
1: water 2: neat (no solvent) View Scheme
参考文献
Ag: MVol.B5, 1.3.2.9, page 73 - 75
反应条件
bis(acetylacetonate)nickel(II); monoethoxy-diethylaluminum T=35°C; other reagents; Rate constant;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 29, # 7 p. 1056 - 1062
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1509 - 1515
反应条件
ethylaluminum dichloride; titanium tetrachloride; triphenylphosphine in benzene T=50°C; Product distribution;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 55, # 7 p. 1756 - 1762
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane in benzene Heatingvarious reaction time; various radicals; various alkenes; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 60, # 12 p. 3826 - 3831
反应条件
lithium in tetrahydrofuran 5 h; HeatingBr-Li exchange; Product distribution;
参考文献
Chemische Berichte, , vol. 118, # 6 p. 2330 - 2342
反应条件
tetrakis(1,3,5-triaza-7-phosphaadamantane)palladium(0) in water T=80°C; 20 h; various catalysts; Product distribution;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 62, # 2 p. 355 - 363