反,反,顺-1,5,9-环十二烷基三烯合成路线 （共 58 条）
参考文献
Liebigs Annalen der Chemie, , vol. 727, p. 143 - 160
反应条件
T=40°C; Oligomerisierung;
参考文献
DE1050333 , ;
DE1056123 , ;
Angewandte Chemie, , vol. 69, p. 397
Journal of Polymer Science, , vol. 38, p. 45
Makromolekulare Chemie, , vol. 69, p. 18,29,30,34
反应条件
T=450°C; other temp. were studied; MechanismProduct distribution;
参考文献
Tetrahedron Letters, , vol. 24, # 21 p. 2143 - 2146
参考文献
Angewandte Chemie, , vol. 69, p. 397
Journal of Polymer Science, , vol. 38, p. 45
DE1043329 , ;
Makromolekulare Chemie, , vol. 69, p. 18,29,30,34
反应条件
T=500°C; other temp. were studied; MechanismProduct distribution;
参考文献
Tetrahedron Letters, , vol. 24, # 21 p. 2143 - 2146
反应条件
Oligomerisierung; Produkt5: Cyclododeca-1c,5c,9t-trien;
参考文献
Angewandte Chemie, , vol. 75, p. 10 - 20
Polymerization and Polycondensation Processes (= Advances in Chemistry Series Nr.34) <Washington 1962>S.137
Journal of the Chemical Society, , p. 1931,1939
Makromolekulare Chemie, , vol. 69, p. 18,29,30,34
反应条件
Oligomerisierung; Einfluss vin Temperatur, Loesungsmittel, Zusammensetzung des Katalysators sowie von Zusaetzen auf diese Reaktion;
参考文献
DE1112069 , ;
Justus Liebigs Annalen der Chemie, , vol. 681, p. 10,19
Makromolekulare Chemie, , vol. 69, p. 18,29,30,34
反应条件
1: 1.) O3/O2, 2.) NaOAc, AcOH, Ac2O / 1.) AcOH, cyclohexane, 5 deg C, 2.) from 30 to 40 deg C, 1.5 h 2: p-toluenesulfonic acid / 24 h / Ambient temperature 3: 90 percent / diisobutylaluminium hydride / diethyl ether; toluene / 1.5 h / -10 °C 4: 100 percent / pyridine / 20 h / 0 °C 5: 1.) CuI / 1.) Et2O, -5 deg C, 40 min, 2.) Et2O, from -5 to 0 deg C, 15 h 6: 95 percent / 10percent aq. HCl / acetone / 6 h 7: 1.) Mg / 1.) THF, 2.) THF, RT, 3 h 8: pyridine / 20 h / 0 °C 9: NaI, Zn / tetrahydrofuran / 3 h / Heating 10: 95 percent / 10percent aq. HCl / acetone / 6 h / 40 °C 11: 95 percent / diisobutylaluminium hydride / diethyl ether; toluene / 1.5 h / -10 °C 12: 75 percent / pyridine View Scheme
参考文献
Odinokov, V. N.; Mukhametzyanova, R. S.; Galeeva, R. I.; Ishmuratov, G. Yu.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 8.1 p. 1399 - 1407
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 8 p. 1619 - 1629
反应条件
1: m-chloroperbenzoic acid 2: magnesium bromide etherate / diethyl ether / Heating View Scheme
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2006/32502 A1, 2006 ;
Location in patent: Page/Page column 67-68 ;
反应条件
1: isopropylbenzene hydroperoxide, MoO2(acac)2, isopropylbenzene / 1 h / 70 °C 2: H2 / Pd/C / ethanol / 50 °C / 30002.4 Torr View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 67, # 6 p. 921 - 926
