反,反,顺-1,5,9-环十二烷基三烯合成路线 （共 58 条）
反应条件
hydrogen T=79.84°C; P=1125.11 Torr;
参考文献
Gaube; David; Sanchayan; Wuchter; Klein
Applied Catalysis A: General, 2011 , vol. 409-410, p. 21 - 27
反应条件
(DHQD)2-PYR; potassium dioxotetrahydroxoosmate(VI); methanesulfonamide; potassium carbonate in water; tert-butyl alcohol T=0°C;
参考文献
Hugger, Uwe
Tetrahedron Letters, 1995 , vol. 36, # 37 p. 6603 - 6606
反应条件
potassium osmate(VI); (DHQD)2-PYR; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III) in water; tert-butyl alcohol T=0°C;
参考文献
Becker, Heinrich; Soler, Marcos A.; Sharpless, K. Barry
Tetrahedron, 1995 , vol. 51, # 5 p. 1345 - 1376
反应条件
cobalt(III) fluoride T=330 - 350°C; 2 h; Yield given;
参考文献
Platonov, V.E.; Prokudin, I.P.; Popkova, N.V.; Rodionov, P.P.; Asovich, V.S.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 10 p. 2205
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 10 p. 2409 - 2410
反应条件
hydrogen T=79.84°C; P=1125.11 Torr;
参考文献
Gaube; David; Sanchayan; Wuchter; Klein
Applied Catalysis A: General, 2011 , vol. 409-410, p. 21 - 27
反应条件
bromine in acetic acid T=20°C; 3 h;
参考文献
Trauer, Heiner; Haufe, Guenter
Zeitschrift fuer Chemie (Stuttgart, Germany), 1988 , vol. 28, # 8 p. 290 - 291
反应条件
1: 1.) O3/O2, 2.) NaOAc, AcOH, Ac2O / 1.) AcOH, cyclohexane, 5 deg C, 2.) from 30 to 40 deg C, 1.5 h 2: p-toluenesulfonic acid / 24 h / Ambient temperature View Scheme
参考文献
Odinokov, V. N.; Mukhametzyanova, R. S.; Galeeva, R. I.; Ishmuratov, G. Yu.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 8.1 p. 1399 - 1407
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 8 p. 1619 - 1629
反应条件
(i) CuSO4, N2H4*H2O, EtOH, (ii) Br2, AcOH, (iii) KOtBu, (MeOCH2CH2)2O; Multistep reaction;
参考文献
Eglinton,G. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 474 - 479
反应条件
bis(cyclopentadienyl)titanium dichloride; tri-isobutyl aluminium
T=190 - 230°C; 0.25 h; isomerization; Product distribution;
参考文献
Zakharkin, L. I.; Zhigareva, G. G.; Pryanishnikov, A. P.; Ovseenko, S. T.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 10 p. 2061 - 2064
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 10 p. 2256 - 2259
反应条件
1.) PPA; palladium on activated charcoal
1.) 190 - 230 deg C, 15 min, 2.) 250 deg C, 10 h; Yield given. Multistep reaction;
参考文献
Zakharkin, L. I.; Zhigareva, G. G.; Pryanishnikov, A. P.; Ovseenko, S. T.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 10 p. 2061 - 2064
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 10 p. 2256 - 2259
