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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
70625-63-7
合成路线
（共 6 条）
70625-63-7
→
反应条件
873443-66-4
反应条件
1: triethylamine / methanol / 66.02 h / 25 °C / |Reflux 2: trichlorophosphate / 10 h / 135 °C View Scheme
参考文献
Harrington, Peter J.; Johnston, Dave; Moorlag, Henk; Wong, Jim-Wah; Hodges, L. Mark; Harris, Les; McEwen, Gerald K.; Smallwood, Blair
Organic Process Research and Development, 2006 , vol. 10, # 6 p. 1157 - 1166
70625-63-7
→
反应条件
342417-01-0
6-(4-甲基哌嗪-1-基)-4-(2-甲基苯基)烟酰胺
反应条件
1: triethylamine / methanol / 66.02 h / 25 °C / |Reflux 2: trichlorophosphate / 10 h / 135 °C 3: methanol / 20.25 h / 18 - 25 °C 4: hydrogen; triethylamine; 20 palladium(II) hydroxide on carbon / methanol / 10 h / 25 °C / 2223.8 - 2497.89 Torr 5: sulfuric acid / toluene / 12 h / 70 °C View Scheme
参考文献
Harrington, Peter J.; Johnston, Dave; Moorlag, Henk; Wong, Jim-Wah; Hodges, L. Mark; Harris, Les; McEwen, Gerald K.; Smallwood, Blair
Organic Process Research and Development, 2006 , vol. 10, # 6 p. 1157 - 1166
70625-63-7
→
反应条件
342417-06-5
反应条件
1: triethylamine / methanol / 66.02 h / 25 °C / |Reflux 2: trichlorophosphate / 10 h / 135 °C 3: methanol / 18.75 h / 18 - 25 °C 4: hydrogen; triethylamine; 20 palladium(II) hydroxide on carbon / methanol / 21 h / 25 °C / 2135.88 - 2482.38 Torr 5: sulfuric acid / toluene / 12 h / 70 °C View Scheme
参考文献
Harrington, Peter J.; Johnston, Dave; Moorlag, Henk; Wong, Jim-Wah; Hodges, L. Mark; Harris, Les; McEwen, Gerald K.; Smallwood, Blair
Organic Process Research and Development, 2006 , vol. 10, # 6 p. 1157 - 1166
70625-63-7
→
反应条件
290297-26-6
奈妥吡坦
反应条件
1: triethylamine / methanol / 66.02 h / 25 °C / |Reflux 2: trichlorophosphate / 10 h / 135 °C 3: methanol / 20.25 h / 18 - 25 °C 4: hydrogen; triethylamine; 20 palladium(II) hydroxide on carbon / methanol / 10 h / 25 °C / 2223.8 - 2497.89 Torr 5: sulfuric acid / toluene / 12 h / 70 °C 6: N-bromosuccinmide / dichloromethane / -5 °C 7: RedAl / toluene / 50 °C 8: N-ethyl-N,N-diisopropylamine / dichloromethane / 40 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 10, # 6 p. 1157 - 1166
70625-63-7
→
反应条件
290296-68-3
2-[3,5-二(三氟甲基)苯基]-N,2-二甲基-N-[4-(2-甲基苯基)-6-吗啉-4-基-吡啶-3-基]丙酰胺
反应条件
1: triethylamine / methanol / 66.02 h / 25 °C / |Reflux 2: trichlorophosphate / 10 h / 135 °C 3: methanol / 18.75 h / 18 - 25 °C 4: sulfuric acid / toluene / 120 h / 70 °C 5: hydrogen; triethylamine; 20 palladium(II) hydroxide on carbon / methanol / 21 h / 25 °C / 1613.54 - 2078.99 Torr 6: N-bromosuccinmide / dichloromethane / -5 °C 7: lithium aluminium tetrahydride / tetrahydrofuran 8: N-ethyl-N,N-diisopropylamine / dichloromethane / 40 °C View Scheme
参考文献
Harrington, Peter J.; Johnston, Dave; Moorlag, Henk; Wong, Jim-Wah; Hodges, L. Mark; Harris, Les; McEwen, Gerald K.; Smallwood, Blair
Organic Process Research and Development, 2006 , vol. 10, # 6 p. 1157 - 1166
70625-63-7
→
反应条件
873443-68-6
反应条件
1: triethylamine / methanol / 66.02 h / 25 °C / |Reflux 2: trichlorophosphate / 10 h / 135 °C 3: methanol / 18.75 h / 18 - 25 °C View Scheme
参考文献
Harrington, Peter J.; Johnston, Dave; Moorlag, Henk; Wong, Jim-Wah; Hodges, L. Mark; Harris, Les; McEwen, Gerald K.; Smallwood, Blair
Organic Process Research and Development, 2006 , vol. 10, # 6 p. 1157 - 1166
