1,4-二氢-2,6-二甲基-4-苯基-3,5-吡啶羧酸二甲酯合成路线 (共 23 条)
反应条件
NbCl5 in acetonitrile T=20°C; 432 h;
参考文献
Filipan-Litvic, Mirela; Litvic, Mladen; Vinkovic, Vladimir
Tetrahedron, 2008 , vol. 64, # 48 p. 10912 - 10918
反应条件
boron trifluoride diethyl etherate in chloroform Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 54, # 17 p. 4134 - 4137
反应条件
boron trifluoride diethyl etherate in chloroform T=0 - 10°C; 3 h; Yields of byproduct given;
参考文献
Hartman, George D.; Phillips, Brian T.; Halczenko, Wasyl; Springer, James P.; Hirshfield, Jordan
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1136 - 1139
反应条件
ammonium acetate
T=90°C; Hantzsch synthesis; 0.916667 h; Neat (no solvent);
参考文献
Koukabi, Nadiya; Kolvari, Eskandar; Zolfigol, Mohammad Ali; Khazaei, Ardeshir; Shaghasemi, Behzad Shirmardi; Fasahati, Behzad
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 10 p. 2001 - 2008
反应条件
ammonium acetate in neat (no solvent)
T=60°C; Hantzsch Dihydropyridine Synthesis; 0.333333 h;
参考文献
Pramanik, Malay; Bhaumik, Asim
Journal of Materials Chemistry A, 2013 , vol. 1, # 37 p. 11210 - 11220
反应条件
p-toluenesulfonic acid sodium salt in water
Hantzsch Dihydropyridine Synthesis; 0.0833333 h; Microwave irradiationRefluxGreen chemistry; Reagent/catalyst;
参考文献
Khadilkar, Bhushan M.; Madyar, Virendra R.
Organic Process Research and Development, 2001 , vol. 5, # 4 p. 452 - 455
反应条件
in dichloromethane
T=40°C; Cycloaddition; addition; 5 h;
参考文献
Palacios, Francisco; Herran, Esther; Rubiales, Gloria
Journal of Organic Chemistry, 1999 , vol. 64, # 17 p. 6239 - 6246
反应条件
sodium butylmonoglycolsulphate in water
0.0833333 h; HeatingIrradiationmicrowave irradiation;
参考文献
Khadilkar, Bhushan M.; Gaikar, Vilas G.; Chitnavis, Ashish A.
Tetrahedron Letters, 1995 , vol. 36, # 44 p. 8083 - 8086
反应条件
1: methanol; 5-acetyl-2,2-dimethyl-[1,3]dioxane-4,6-dione Microwave irradiation;
2: benzaldehyde With ammonium acetate in methanol
Microwave irradiation;
参考文献
More; Mahulikar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2011 , vol. 50, # 5 p. 745 - 747
反应条件
organosulfonic acid 15-functionalized periodic mesoporous organosilicas in neat (no solvent)
T=90°C; 1.5 h;
参考文献
Karimi, Babak; Mobaraki, Akbar; Mirzaei, Hamid M.; Zareyee, Daryoush; Vali, Hojatollah
ChemCatChem, 2014 , vol. 6, # 1 p. 212 - 219