3-氨基-5-溴苯甲酸甲酯合成路线 （共 5 条）
反应条件
1: With hydrogenchloride; iron in ethanol; water 5 h; Reflux; 2: With sodium carbonate in methanol; water
参考文献
Kakuta, Hiroki; Azumaya, Isao; Masu, Hyuma; Matsumura, Mio; Yamaguchi, Kentaro; Kagechika, Hiroyuki; Tanatani, Aya
Tetrahedron, 2010 , vol. 66, # 42 p. 8254 - 8260
反应条件
thionyl chloride T=0 - 20°C;
参考文献
Broch, Sidonie; Heenon, Helne; Debaud, Anne-Laure; Fogeron, Marie-Laure; Bonnefoy-Berard, Nathalie; Anizon, Fabrice; Moreau, Pascale
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 19 p. 7132 - 7143
反应条件
1: Br2; Ag2SO4; conc. H2SO4 2: SnCl2*2H2O / ethanol View Scheme
参考文献
Tetrahedron Letters, , vol. 44, # 7 p. 1469 - 1472
反应条件
1: thionyl chloride / 6 h / 0 °C / Reflux 2: tin(ll) chloride / tetrahydrofuran; ethanol / 6 h / 0 °C / Reflux View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 8 p. 2471 - 2478
反应条件
1: With sulfuric acid in water T=0°C; Cooling with ice; 2: With sodium nitrite in water T=0°C; 0.5 h; Cooling with iceReflux;
参考文献
Journal of the American Chemical Society, , vol. 135, # 46 p. 17408 - 17416
