1: 67 percent / 4-(dimethylamino)pyridine / CH2Cl2 / 20 °C 2: acetonitrile / 20 °C / UV-irradiation View Scheme
参考文献
Najiwara, Toshihiro; Hashimoto, Ji-ichiro; Segawa, Katsunori; Sakuragi, Hirochika
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 3 p. 575 - 585
Bretscher; Rule; Spence
Journal of the Chemical Society, 1928 , p. 1500
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Najiwara, Toshihiro; Hashimoto, Ji-ichiro; Segawa, Katsunori; Sakuragi, Hirochika
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 3 p. 575 - 585
ethylaluminum dichloride in dichloromethane; toluene
T=-78 - 20°C; Yield given;
参考文献
Eissenstat, Michael A.; Bell, Malcolm R.; D'Ambra, Thomas E.; Alexander, E. John; Daum, Sol J.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 16 p. 3094 - 3105
4-(N,N-dimethlyamino)pyridine in dichloromethane
T=20°C;
参考文献
Najiwara, Toshihiro; Hashimoto, Ji-ichiro; Segawa, Katsunori; Sakuragi, Hirochika
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 3 p. 575 - 585