1-氯-3,5-二甲基金刚烷合成路线 （共 8 条）
反应条件
hydrogenchloride in water T=25 - 30°C; 15 h;
参考文献
Reddy, Jambula Mukunda; Prasad, Ganji; Raju, Veeramalla; Ravikumar, Mylavarapu; Himabindu, Vurumidi; Reddy, Ghanta Mahesh
Organic Process Research and Development, 2007 , vol. 11, # 2 p. 268 - 269
反应条件
1: bromine; water / 25 °C / |Reflux 2: hydrogenchloride / water / 15 h / 25 - 30 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 11, # 2 p. 268 - 269
参考文献
Zhurnal Organicheskoi Khimii, , vol. 2, # 9 p. 1612 - 1615,1590 - 1592
反应条件
di-tert-butyl peroxide; (chloromethyl)methyldichlorosilane in neat (no solvent) T=170°C; 2 h; Product distributionMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 57, # 11 p. 2537 - 2540,2258 - 2261
反应条件
hydrogenchloride; sodium hydroxide; urea in water
参考文献
Merz and Co.
Patent: US4122193 A1, 1978 ;
参考文献
Reddy, Jambula Mukunda; Prasad, Ganji; Raju, Veeramalla; Ravikumar, Mylavarapu; Himabindu, Vurumidi; Reddy, Ghanta Mahesh
Organic Process Research and Development, 2007 , vol. 11, # 2 p. 268 - 269
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane in toluene Heating;
参考文献
Ballestri, M.; Chatgilialoglu, C.; Clark, K. B.; Griller, D.; Giese, B.; Kopping, B.
Journal of Organic Chemistry, 1991 , vol. 56, # 2 p. 678 - 683
反应条件
1: With sulfuric acid in acetic acid T=20 - 75°C; Ritter Reaction; 4 h; 2: With water in acetic acid; toluene T=5 - 25°C; 0.75 h;
参考文献
A.M.S.A. ANONIMA MATERIE SINTETICHE E AFFINI S.p.A.
Patent: EP1721888 A1, 2006 ;
Location in patent: Page/Page column 7; 13 ;
