4,5,6,7-四甲基-1H-茚合成路线 （共 10 条）
反应条件
toluene-4-sulfonic acid in toluene
Dehydration; 5 h; Heating;
参考文献
Ready, Thomas E.; Chien, James C.W.; Rausch, Marvin D.
Journal of Organometallic Chemistry, 1999 , vol. 583, # 1-2 p. 11 - 27
反应条件
1,2-bis(4-methoxyphenyl)diazene in tetrahydrofuran
T=60°C; 5 h;
参考文献
Takahashi, Tamotsu; Song, Zhiyi; Hsieh, Yi-Fang; Nakajima, Kiyohiko; Kanno, Ken-Ichiro
Journal of the American Chemical Society, 2008 , vol. 130, # 46 p. 15236 - 15237
反应条件
Azobenzene in tetrahydrofuran
T=60°C; 5 h;
参考文献
Takahashi, Tamotsu; Song, Zhiyi; Hsieh, Yi-Fang; Nakajima, Kiyohiko; Kanno, Ken-Ichiro
Journal of the American Chemical Society, 2008 , vol. 130, # 46 p. 15236 - 15237
反应条件
aluminum oxide in benzene
T=420°C;
参考文献
Klemm,L.H. et al.
Journal of Organic Chemistry, 1974 , vol. 39, p. 698 - 701
反应条件
1: 82 percent / LiAlH4 / diethyl ether / Heating
2: 81 percent / p-toluenesulfonic acid / toluene / 5 h / Heating
View Scheme
参考文献
Ready, Thomas E.; Chien, James C.W.; Rausch, Marvin D.
Journal of Organometallic Chemistry, 1999 , vol. 583, # 1-2 p. 11 - 27
反应条件
aluminum oxide
T=250°C; P=12 Torr;
参考文献
Criegee,R. et al.
Chemische Berichte, 1964 , vol. 97, p. 3461 - 3468
反应条件
1: AlCl3 / CH2Cl2
2: (decarboxylation)
3: LiAlH4 / diethyl ether
4: oxalic acid / H2O / Heating
View Scheme
参考文献
Marechal,E. et al.
Bulletin de la Societe Chimique de France, 1968 , p. 2049 - 2053
反应条件
1: (decarboxylation)
2: LiAlH4 / diethyl ether
3: oxalic acid / H2O / Heating
View Scheme
参考文献
Marechal,E. et al.
Bulletin de la Societe Chimique de France, 1968 , p. 2049 - 2053
反应条件
1: AlCl3 / CS2
2: H2SO4
3: LiAlH4 / diethyl ether
4: Al2O3 / 150 °C / 12 Torr
View Scheme
参考文献
Criegee,R. et al.
Chemische Berichte, 1964 , vol. 97, p. 3461 - 3468
反应条件
1: H2SO4
2: LiAlH4 / diethyl ether
3: Al2O3 / 150 °C / 12 Torr
View Scheme
参考文献
Criegee,R. et al.
Chemische Berichte, 1964 , vol. 97, p. 3461 - 3468
