2-氯-2-膦酰基乙酸三乙酯合成路线 (共 19 条)
反应条件
sodium sulfite in ethanol; water 0.333333 h; Ambient temperature;
参考文献
McKenna, Charles E.; Khawli, Leslie A.
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5467 - 5471
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane T=-78°C; 0.5 h;
参考文献
Teulade, Marie Paule; Savignac, Philippe; Aboujaoude, Elie Elia; Collignon, Noel
Journal of Organometallic Chemistry, 1985 , vol. 287, p. 145 - 156
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 32, p. 2994 - 3001,2945 - 2950
反应条件
[Me4N][BF4]; 4-methoxy-benzaldehyde in N,N-dimethyl-formamide Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1332 - 1343
反应条件
[Me4N][BF4]; 4-methoxy-benzaldehyde in N,N-dimethyl-formamide Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag; Yields of byproduct given;
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
sulfuryl dichloride Chlorination;
参考文献
Krawczyk; Koszuk; Bodalski
Polish Journal of Chemistry, 2000 , vol. 74, # 8 p. 1123 - 1128
反应条件
[Me4N][BF4] in N,N-dimethyl-formamide Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag; Yield given;
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
[Me4N][BF4] in N,N-dimethyl-formamide Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag; Yield given;
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
(i) nBuLi, (ii) aq. HCl; Multistep reaction;
参考文献
Tetrahedron Letters, , p. 2913 - 2914
反应条件
(i) nBuLi, THF, hexane, (ii) /BRN= 385653/; Multistep reaction;
参考文献
Synthesis, , p. 31 - 33