2-氯-2-膦酰基乙酸三乙酯合成路线 （共 19 条）
反应条件
(i) NaH, Et2O, (ii) /BRN= 1761567/; Multistep reaction;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 693, p. 134 - 157
反应条件
1: K2CO3 / tetrahydrofuran 2: 10 percent / Me4NBF4 / dimethylformamide / Ambient temperature; controlled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag View Scheme
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
[Me4N][BF4]; 4-methoxy-benzaldehyde in N,N-dimethyl-formamide Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag; Yields of byproduct given;
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
[Me4N][BF4] in N,N-dimethyl-formamide Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag; Yield given;
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
[Me4N][BF4] in N,N-dimethyl-formamide Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag; Yield given;
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
sodium hypobromide in water
参考文献
Journal of Organic Chemistry, , vol. 51, # 26 p. 5467 - 5471
反应条件
[Me4N][BF4]; Azobenzene in N,N-dimethyl-formamide Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag;
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
[Me4N][BF4] in N,N-dimethyl-formamide Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag; Yield given;
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
1: 82 percent / KOH / ethanol; H2O / 24 h / 20 °C
2: 72 percent / piperidine / ethanol / Heating
View Scheme
参考文献
Krawczyk; Koszuk; Bodalski
Polish Journal of Chemistry, 2000 , vol. 74, # 8 p. 1123 - 1128
