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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
70711-49-8
合成路线
（共 9 条）
518333-30-7
→
反应条件
70711-49-8
反应条件
hydrogenchloride in tetrahydrofuran Heating;
参考文献
Kikuchi, Haruhisa; Sasaki, Kazunori; Sekiya, Jun'ichi; Maeda, Yasuo; Amagai, Aiko; Kubohara, Yuzuru; Oshima, Yoshiteru
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 12 p. 3203 - 3214
1611-56-9
11-溴-1-十一醇
→
反应条件
70711-49-8
反应条件
1.1: 96 percent / LiBr; p-toluenesulfonic acid / 16 h / 20 °C 2.1: NH3; Li / dimethylsulfoxide / -78 - 25 °C 2.2: 98 percent / dimethylsulfoxide / 1 h / -78 - 25 °C 3.1: n-BuLi / tetrahydrofuran / 0.08 h / 0 °C 3.2: 61 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / 0 - 20 °C 4.1: 80 percent / NH3; Na / tetrahydrofuran / -78 - -33 °C 5.1: HCl / methanol / 16 h / 25 °C View Scheme
参考文献
Villorbina, Gemma; Roura, Lidia; Camps, Francisco; Joglar, Jesus; Fabrias, Gemma
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2820 - 2829
136667-40-8
→
反应条件
70711-49-8
反应条件
1.1: NH3; Li / dimethylsulfoxide / -78 - 25 °C 1.2: 98 percent / dimethylsulfoxide / 1 h / -78 - 25 °C 2.1: n-BuLi / tetrahydrofuran / 0.08 h / 0 °C 2.2: 61 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / 0 - 20 °C 3.1: 80 percent / NH3; Na / tetrahydrofuran / -78 - -33 °C 4.1: HCl / methanol / 16 h / 25 °C View Scheme
参考文献
Villorbina, Gemma; Roura, Lidia; Camps, Francisco; Joglar, Jesus; Fabrias, Gemma
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2820 - 2829
518333-18-1
→
反应条件
70711-49-8
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.08 h / 0 °C 1.2: 61 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / 0 - 20 °C 2.1: 80 percent / NH3; Na / tetrahydrofuran / -78 - -33 °C 3.1: HCl / methanol / 16 h / 25 °C View Scheme
参考文献
Villorbina, Gemma; Roura, Lidia; Camps, Francisco; Joglar, Jesus; Fabrias, Gemma
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2820 - 2829
518333-20-5
→
反应条件
70711-49-8
反应条件
1: 80 percent / NH3; Na / tetrahydrofuran / -78 - -33 °C 2: HCl / methanol / 16 h / 25 °C View Scheme
参考文献
Villorbina, Gemma; Roura, Lidia; Camps, Francisco; Joglar, Jesus; Fabrias, Gemma
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2820 - 2829
736177-61-0
→
反应条件
70711-49-8
反应条件
1.1: SO3*pyridine / tetrahydrofuran / 20 °C 1.2: 67 percent / LiAlH4 / tetrahydrofuran / 20 °C 2.1: 92 percent / hydrochloric acid / tetrahydrofuran / Heating View Scheme
参考文献
Kikuchi, Haruhisa; Sasaki, Kazunori; Sekiya, Jun'ichi; Maeda, Yasuo; Amagai, Aiko; Kubohara, Yuzuru; Oshima, Yoshiteru
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 12 p. 3203 - 3214
736177-59-6
→
反应条件
70711-49-8
反应条件
1.1: 90 percent / DIBAL-H / CH2Cl2; toluene / 1 h / -20 °C 2.1: SO3*pyridine / tetrahydrofuran / 20 °C 2.2: 67 percent / LiAlH4 / tetrahydrofuran / 20 °C 3.1: 92 percent / hydrochloric acid / tetrahydrofuran / Heating View Scheme
参考文献
Kikuchi, Haruhisa; Sasaki, Kazunori; Sekiya, Jun'ichi; Maeda, Yasuo; Amagai, Aiko; Kubohara, Yuzuru; Oshima, Yoshiteru
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 12 p. 3203 - 3214
5675-51-4
1,12-十二烷二醇
→
反应条件
70711-49-8
反应条件
1.1: 40 percent / N-ethyldiisopropylamine / CH2Cl2 / 20 °C 2.1: PCC / CH2Cl2 / 3 h / 20 °C 3.1: NaH / benzene / 20 °C 4.1: 90 percent / DIBAL-H / CH2Cl2; toluene / 1 h / -20 °C 5.1: SO3*pyridine / tetrahydrofuran / 20 °C 5.2: 67 percent / LiAlH4 / tetrahydrofuran / 20 °C 6.1: 92 percent / hydrochloric acid / tetrahydrofuran / Heating View Scheme
参考文献
Kikuchi, Haruhisa; Sasaki, Kazunori; Sekiya, Jun'ichi; Maeda, Yasuo; Amagai, Aiko; Kubohara, Yuzuru; Oshima, Yoshiteru
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 12 p. 3203 - 3214
518333-10-3
→
反应条件
70711-49-8
反应条件
1.1: NaH / benzene / 20 °C 2.1: 90 percent / DIBAL-H / CH2Cl2; toluene / 1 h / -20 °C 3.1: SO3*pyridine / tetrahydrofuran / 20 °C 3.2: 67 percent / LiAlH4 / tetrahydrofuran / 20 °C 4.1: 92 percent / hydrochloric acid / tetrahydrofuran / Heating View Scheme
参考文献
Kikuchi, Haruhisa; Sasaki, Kazunori; Sekiya, Jun'ichi; Maeda, Yasuo; Amagai, Aiko; Kubohara, Yuzuru; Oshima, Yoshiteru
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 12 p. 3203 - 3214
