2,2-二溴-4,4-二-叔丁基-1,1-联苯合成路线 (共 8 条)
反应条件
aluminium trichloride in benzene
参考文献
Journal of Organic Chemistry, , vol. 44, p. 3037 - 3041
反应条件
1: With magnesium in tetrahydrofuran; ethylene dibromide T=20°C; 16 h; 2: With (teeda)*H2SiCl2 in tetrahydrofuran; dichloromethane T=20°C; 48 h;
参考文献
Corey, Joyce Y.; Trankler, Kevin A.; Braddock-Wilking, Janet; Rath, Nigam P.
Organometallics, 2010 , vol. 29, # 21 p. 5708 - 5713
反应条件
water; magnesium; ethylene dibromide in tetrahydrofuran T=74.7°C; variation of reagent and conditions; Product distribution;
参考文献
Corey, Joyce Y.; Chang, Lihsueh S.
Journal of Organometallic Chemistry, 1986 , vol. 307, p. 7 - 14
反应条件
magnesium; ethylene dibromide in tetrahydrofuran T=74.7°C; variation of reagent and conditions; Product distribution;
参考文献
Corey, Joyce Y.; Chang, Lihsueh S.
Journal of Organometallic Chemistry, 1986 , vol. 307, p. 7 - 14
反应条件
1: With magnesium in tetrahydrofuran; ethylene dibromide 0.5 h; 2: With (teeda)*H2SiCl2 in tetrahydrofuran; dichloromethane; ethylene dibromide
参考文献
Corey, Joyce Y.; Trankler, Kevin A.; Braddock-Wilking, Janet; Rath, Nigam P.
Organometallics, 2010 , vol. 29, # 21 p. 5708 - 5713
反应条件
bromine; iron in tetrachloromethane
T=29 - 30°C; 3.3 h;
参考文献
Corey, Joyce Y.; Chang, Lihsueh S.
Journal of Organometallic Chemistry, 1986 , vol. 307, p. 7 - 14
反应条件
n-butyllithium; potassium tert-butylate; bromine in hexane
参考文献
Schlosser, Manfred; Mangano, Guiseppe; Leroux, Frederic
European Journal of Organic Chemistry, 2004 , # 5 p. 1014 - 1017
反应条件
water; magnesium; ethylene dibromide in tetrahydrofuran
T=74.7°C; variation of reagent and conditions; Product distribution;
参考文献
Corey, Joyce Y.; Chang, Lihsueh S.
Journal of Organometallic Chemistry, 1986 , vol. 307, p. 7 - 14