3-甲基异恶唑-5-甲醛合成路线 （共 12 条）
反应条件
sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine in dichloromethane T=0°C; 1 h;
参考文献
Salmon, Anne; Carboni, Bertrand
Journal of Organometallic Chemistry, 1998 , vol. 567, # 1-2 p. 31 - 37
反应条件
diisobutylaluminium hydride in hexane T=-65°C; 2 h;
参考文献
Bell, David; Crowe, Eleanor A.; Dixon, Nicholas J.; Geen, Graham R.; Mann, Inderjit S.; Shipton, Mark R.
Tetrahedron, 1994 , vol. 50, # 22 p. 6643 - 6652
反应条件
1: 57 percent / citric acid / methanol / 4 h / Ambient temperature 2: 85 percent / DMSO, triethylamine, sulfur trioxide-pyridine complex / CH2Cl2 / 1 h / 0 °C View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 567, # 1-2 p. 31 - 37
反应条件
sodium ethanolate T=180°C;
参考文献
Gazzetta Chimica Italiana, , vol. 72, p. 99,106
反应条件
sodium hydroxide Erwaermen des entstandenen Acetonitriloxids in Aether mit Propiolaldehyd;
参考文献
Atti della Societa Peloritana di Scienze Fisiche, Matematiche e Naturali, , vol. 5, p. 159,167
反应条件
ethanol; hydroxylamine Erhitzen des Reaktionsprodukts mit wss. HCl;
参考文献
Gazzetta Chimica Italiana, , vol. 73, p. 99,103
反应条件
1: diethyl ether; hydroxylamine hydrochloride 2: aqueous HCl 3: ethanolic sodium ethylate / 180 °C View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 72, p. 99,106
反应条件
potassium dichromate; sulfuric acid
参考文献
Gazzetta Chimica Italiana, , vol. 69, p. 536,541
反应条件
beim Kochen des Reaktionsprodukts mit verd. HCl;
参考文献
Gazzetta Chimica Italiana, , vol. 73, p. 99,103
反应条件
potassium dichromate; sulfuric acid
参考文献
Panizzi
Gazzetta Chimica Italiana, 1942 , vol. 72, p. 99,106
