4-苯基亚甲基-2,6-二叔丁基-2,5-环己二烯-1-酮合成路线 （共 6 条）
反应条件
C5CoN5O2(3-)*3C36H30NP2(1+) in dichloromethane T=0°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 21, p. 4849 - 4852
反应条件
piperidine in butan-1-ol
24 h; Reflux;
参考文献
Hakuto Co., Ltd
Patent: EP1604965 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
chloro-trimethyl-silane in dichloromethane
3 h;
参考文献
Goulart, Marilia O. F.; Utley, James H. P.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2520 - 2525
反应条件
1: 59 percent / tetrahydrofuran; diethyl ether; cyclohexane
2: 81 percent / trimethylsilyl chloride / CH2Cl2 / 3 h
View Scheme
参考文献
Goulart, Marilia O. F.; Utley, James H. P.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2520 - 2525
反应条件
1: 59 percent / tetrahydrofuran; diethyl ether; cyclohexane
2: 81 percent / trimethylsilyl chloride / CH2Cl2 / 3 h
View Scheme
参考文献
Goulart, Marilia O. F.; Utley, James H. P.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2520 - 2525
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in benzene
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 66 - 78
