N-(4-甲基苯基)-1,3-苯并噻唑-2-胺合成路线 (共 12 条)
反应条件
1,10-phenanthroline; sodium hydrogencarbonate in water
T=80°C; 2 h;
参考文献
Zhang, Wu; Yue, Yun; Yu, Dan; Song, Lei; Xu, Yang-Yang; Tian, Yu-Jie; Guo, Yu-Jun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 11-12 p. 2283 - 2287
反应条件
1,4-diaza-bicyclo[2.2.2]octane in toluene
T=60°C; 8 h;
参考文献
Yang, Jin; Li, Pinhua; Wang, Lei
Tetrahedron, 2011 , vol. 67, # 31 p. 5543 - 5549
反应条件
1: T=20°C; 0.5 h;
2: With potassium carbonate in dimethyl sulfoxide
T=110°C; 5 h;
参考文献
Mirza, Behrooz; Mirzazadeh, Roghieh; Zeeb, Mohsen
Journal of Chemical Research, 2013 , vol. 37, # 12 p. 778 - 779
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dimethyl sulfoxide
T=20°C; 24 h;
参考文献
Wang, Rui; Yang, Wen-Juan; Yue, Liang; Pan, Wei; Zeng, Hong-Yao
Synlett, 2012 , vol. 23, # 11 p. 1643 - 1648
反应条件
t-Bu Brett Phos; water; palladium diacetate; potassium carbonate in tert-butyl alcohol
T=110°C; 5 h; Inert atmosphere;
参考文献
McGowan, Meredeth A.; Henderson, Jaclyn L.; Buchwald, Stephen L.
Organic Letters, 2012 , vol. 14, # 6 p. 1432 - 1435
反应条件
iron(III) sulphate monohydrate; DABCO*6H2O; silica gel
T=80°C; Inert atmosphereneat (no solvent);
参考文献
Ding, Qiuping; Cao, Banpeng; Yang, Qin; Liu, Xianjin; Peng, Yiyuan
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 8 p. 1782 - 1789
反应条件
potassium carbonate; copper(II) oxide in dimethyl sulfoxide
T=80°C; 8 h;
参考文献
Saha, Prasenjit; Ramana, Tamminana; Purkait, Nibadita; Ali, Md. Ashif; Paul, Rajesh; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8719 - 8725
反应条件
1,1'-(ethane-1,2-diyl)dipyridinium ditribromide; triethylamine in acetonitrile
T=20°C;
参考文献
Yella, Ramesh; Patel, Bhisma K.
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 5 p. 754 - 763
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dimethyl sulfoxide
T=20°C; 24 h;
参考文献
Wang, Rui; Yang, Wen-Juan; Yue, Liang; Pan, Wei; Zeng, Hong-Yao
Synlett, 2012 , vol. 23, # 11 p. 1643 - 1648
反应条件
in chloroform
T=47 - 50°C; 0.333333 h;
参考文献
L'abbe, Gerrit; Franek, Walter; Toppet, Suzanne; Delbeke, Pieter
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 4 p. 923 - 925