6-甲基-2,4-蝶啶二胺合成路线 （共 26 条）
反应条件
piperidine in water
550 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zav'yalov, S. I.; Zavozin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 7 p. 1355 - 1357
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 7 p. 1666 - 1668
反应条件
piperidine in water
240 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zav'yalov, S. I.; Zavozin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 7 p. 1355 - 1357
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 7 p. 1666 - 1668
反应条件
sodium hydroxide
pH 8;
参考文献
Sato et al.
Nippon Kagaku Zasshi, 1951 , vol. 72, p. 866
Chem.Abstr., 1953 , p. 5946
反应条件
potassium permanganate
1.) 170 deg C, 2.) aq. AcOH, 20 deg C, 2 h;
参考文献
Zav'yalov, S. I.; Zavolin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1700 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 8 p. 1910 - 1913
反应条件
sodium hydrogensulfite in water
T=80°C; 5.5 h; further cyclizating agents; Product distribution;
参考文献
Zav'yalov, S. I.; Zavoshin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 2 p. 419 - 422
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 2 p. 452 - 455
反应条件
550 h; Product distribution;
参考文献
Zav'yalov, S. I.; Zavolin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1700 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 8 p. 1910 - 1913
反应条件
170 h; Product distribution;
参考文献
Zav'yalov, S. I.; Zavolin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1700 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 8 p. 1910 - 1913
反应条件
170 h; Product distribution;
参考文献
Zav'yalov, S. I.; Zavolin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1700 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 8 p. 1910 - 1913
反应条件
290 h; Product distribution;
参考文献
Zav'yalov, S. I.; Zavolin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1700 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 8 p. 1910 - 1913
反应条件
170 h; Product distribution;
参考文献
Zav'yalov, S. I.; Zavolin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1700 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 8 p. 1910 - 1913
