(1-苄基-1H-吡唑-4-基)-甲醇合成路线 （共 5 条）
反应条件
thionyl chloride in dichloromethane T=20°C; 5 h;
参考文献
WO2005/68432 A1, ;
Page/Page column 186 ;
反应条件
1: With Dess-Martin periodane in dichloromethane T=20°C; 1.5 h; 2: With water; sodium hydrogencarbonate; sodium thiosulfate in dichloromethane T=20°C; 0.5 h;
参考文献
SEPRACOR INC.
Patent: US2008/4327 A1, 2008 ;
Location in patent: Page/Page column 76 ;
参考文献
Jones et al.
Journal of the American Chemical Society, 1949 , vol. 71, p. 4000
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C; 1.58333 h;
2: With hydrogenchloride; water in tetrahydrofuran
参考文献
SEPRACOR INC.
Patent: US2008/4327 A1, 2008 ;
Location in patent: Page/Page column 75-76 ;
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C; 5.5 h;
2: With potassium hydroxide; water in tetrahydrofuran
T=0°C;
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: WO2005/68432 A1, 2005 ;
Location in patent: Page/Page column 185-186 ;
