5-O-苯甲酰基-2,3-脱水胸腺嘧啶脱氧核苷合成路线 （共 9 条）
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in N,N-dimethyl-formamide 1 h; Ambient temperature;
参考文献
Becouarn; Czernecki; Valery
Nucleosides and Nucleotides, 1995 , vol. 14, # 6 p. 1227 - 1232
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in N,N-dimethyl-formamide T=125 - 130°C; 2.5 h;
参考文献
Chen, Bang-Chi; Quinlan, Sandra L.; Reid, J. Gregory
Tetrahedron Letters, 1995 , vol. 36, # 44 p. 7961 - 7964
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetone
参考文献
Tetrahedron Letters, , vol. 36, # 44 p. 7961 - 7964
反应条件
sodium azide in water; N,N-dimethyl-formamide
参考文献
Korchevskaya; Ostrovskii; Malin; Trukhanovich; Shcherbinin
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 5 p. 735 - 737
反应条件
in 1,4-dioxane; N,N-dimethyl-formamide T=100°C; Kinetics; Further Variations:Solvents;
参考文献
Korchevskaya; Malin; Shcherbinin; Ostrovskii
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 9 p. 1369 - 1372
反应条件
1: NaN3 / dimethylformamide; H2O 2: 71 percent / NaOMe / methanol View Scheme
参考文献
Chen, Bang-Chi; Quinlan, Sandra L.; Reid, J. Gregory
Tetrahedron Letters, 1995 , vol. 36, # 44 p. 7961 - 7964
反应条件
1: 96 percent / dimethylformamide / 1 h / 140 °C 2: 88 percent / AcOH, 30percent H2O2 / tetrahydrofuran / 3 h / Ambient temperature 3: 92 percent / 1M NaOMe / methanol / Ambient temperature View Scheme
参考文献
Becouarn; Czernecki; Valery
Nucleosides and Nucleotides, 1995 , vol. 14, # 6 p. 1227 - 1232
反应条件
sodium methylate in methanol Ambient temperature;
参考文献
Czernecki; Valery
Journal of the Chemical Society - Series Chemical Communications, 1990 , # 11 p. 801 - 802
反应条件
1: 96 percent / dimethylformamide / 1 h / 140 °C
2: 88 percent / AcOH, 30percent H2O2 / tetrahydrofuran / 3 h / Ambient temperature
View Scheme
参考文献
Becouarn; Czernecki; Valery
Nucleosides and Nucleotides, 1995 , vol. 14, # 6 p. 1227 - 1232
