N-(三甲氧基甲硅烷基丙基)咪唑合成路线 (共 3 条)
反应条件
in tetrahydrofuran
T=66°C; 13 h;
参考文献
Cazin, Catherine S. J.; Veith, Michael; Braunstein, Pierre; Bedford, Robin B.
Synthesis, 2005 , # 4 art. no. Z17204SS, p. 622 - 626
反应条件
1: 1H-imidazole With sodium hydride in tetrahydrofuran
Inert atmosphere;
2: (3-chloropropyl)trimethoxysilane in tetrahydrofuran
30 h; RefluxInert atmosphere;
参考文献
Karimi, Babak; Gholinejad, Mohammad; Khorasani, Mojtaba
Chemical Communications, 2012 , vol. 48, # 71 p. 8961 - 8963
反应条件
1: 1H-imidazole With sodium hydride in tetrahydrofuran
Inert atmosphereCooling;
2: (γ-iodopropyl)trimethoxysilane in tetrahydrofuran
Inert atmosphereReflux;
参考文献
Litschauer, Marco; Neouze, Marie-Alexandra
Journal of Materials Chemistry, 2008 , vol. 18, # 6 p. 640 - 646