1-(碘甲基)-4-甲氧基苯合成路线 （共 24 条）
反应条件
pyridine; tributyltin chloride T=50°C; Δ G; Thermodynamic dataEquilibrium constant;
参考文献
Friedrich, Edwin C.; Abma, Charles B.
Journal of the American Chemical Society, 1980 , vol. 102, # 4 p. 1367 - 1371
反应条件
pyridine; tri-n-butyltin bromide T=50°C; Δ G; Thermodynamic data;
参考文献
Friedrich, Edwin C.; Abma, Charles B.
Journal of the American Chemical Society, 1980 , vol. 102, # 4 p. 1367 - 1371
反应条件
1: 1) LiN(SiMe3)2 / 1) THF, -76 deg C, 20 min, 2) -76 deg C to RT, overnight 2: 77 percent / HOAc, conc. aq. HCl / 2 h / Heating View Scheme
参考文献
Seebach, Dieter; Gees, Thomas; Schuler, Franz
Liebigs Annalen der Chemie, 1993 , # 7 p. 785 - 800
反应条件
diiodo monosilane in dichloromethane
T=22°C; 0.0833333 h; 150 molpercent DIS;
参考文献
Keinan, E.; Perez, D.; Sahai, M.; Shvily, R.
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2927 - 2938
反应条件
Amberlyst 15; sodium iodide in acetonitrile
T=20°C; 0.75 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Jamalian, Arezu; Kazemi, Foad
Tetrahedron, 2005 , vol. 61, # 23 p. 5699 - 5704
反应条件
sodium iodide; triethylamine in N-methyl-acetamide; dichloromethane; ethyl acetate
参考文献
Shionogi and Co., Ltd.
Patent: US4504658 A1, 1985 ;
反应条件
APDPP; N-iodo-succinimide in dichloromethane
1.5 h; Heating;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Gholinejad, Mohammad
Canadian Journal of Chemistry, 2006 , vol. 84, # 7 p. 1006 - 1012
反应条件
APDPP; iodine in dichloromethane
T=20°C;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Gholinejad, Mohammad
Canadian Journal of Chemistry, 2006 , vol. 84, # 7 p. 1006 - 1012
反应条件
tetrachlorosilane; sodium iodide in acetonitrile
T=20°C; 1.25 h;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Tetrahedron Letters, 2002 , vol. 43, # 40 p. 7139 - 7141
反应条件
iodine; triphenylphosphine in dichloromethane
T=20°C; 48 h;
参考文献
Alvarez-Manzaneda; Chahboun; Cabrera Torres; Alvarez; Haidour; Ramos Lopez
Tetrahedron Letters, 2005 , vol. 46, # 21 p. 3755 - 3759
