1-(碘甲基)-4-甲氧基苯合成路线 （共 24 条）
反应条件
sodium iodide in acetone
T=20°C; 1.5 h;
参考文献
Bilodeau, Francois; Dube, Laurence; Deslongchamps, Pierre
Tetrahedron, 2003 , vol. 59, # 16 p. 2781 - 2791
反应条件
diiodo monosilane in dichloromethane
0.0333333 h; Ambient temperature;
参考文献
Keinan, E.; Perez, D.; Sahai, M.; Shvily, R.
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2927 - 2938
反应条件
triethylamine in dichloromethane; N,N-dimethyl-formamide
参考文献
Schering Corporation
Patent: US5225436 A1, 1993 ;
反应条件
tetra-(n-butyl)ammonium iodide; [bmim][InCl4]
T=135 - 140°C; 0.0916667 h; Microwave irradiationNeat (no solvent); chemoselective reaction;
参考文献
Mirjafari, Arsalan; Mohammadpoor-Baltork, Iraj; Moghadam, Majid; Tangestaninejad, Shahram; Mirkhani, Valiollah; Khosropour, Ahmad Reza
Tetrahedron Letters, 2010 , vol. 51, # 25 p. 3274 - 3276
反应条件
tetra-(n-butyl)ammonium iodide; [bmim][InCl4]
T=135 - 140°C; 0.0916667 h; Microwave irradiationNeat (no solvent); chemoselective reaction;
参考文献
Mirjafari, Arsalan; Mohammadpoor-Baltork, Iraj; Moghadam, Majid; Tangestaninejad, Shahram; Mirkhani, Valiollah; Khosropour, Ahmad Reza
Tetrahedron Letters, 2010 , vol. 51, # 25 p. 3274 - 3276
反应条件
diiodo monosilane in chloroform-d1
T=22°C;
参考文献
Keinan, E.; Perez, D.; Sahai, M.; Shvily, R.
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2927 - 2938
参考文献
Lorenzo, A.; Molina, P.; Vilaplana, M. J.
Synthesis, 1980 , # 10 p. 853 - 854
反应条件
pyridine; Bu3SnI
T=50°C; Δ G; Thermodynamic dataEquilibrium constant;
参考文献
Friedrich, Edwin C.; Abma, Charles B.
Journal of the American Chemical Society, 1980 , vol. 102, # 4 p. 1367 - 1371
反应条件
1: 72 percent / benzene / Ambient temperature
2: 78 percent / 1 Torr
View Scheme
参考文献
Lorenzo, A.; Molina, P.; Vilaplana, M. J.
Synthesis, 1980 , # 10 p. 853 - 854
反应条件
1: 73 percent / methanol / 3 h / Heating
2: 72 percent / benzene / Ambient temperature
3: 78 percent / 1 Torr
View Scheme
参考文献
Lorenzo, A.; Molina, P.; Vilaplana, M. J.
Synthesis, 1980 , # 10 p. 853 - 854
