2-氰基-3-苯丙烯酰胺合成路线 (共 17 条)
反应条件
ammonium sulphamate Knoevenagel condensation; 0.00416667 h; Microwave irradiationneat (no solvent);
参考文献
Mogilaiah; Babu, H. Sharath; Vidya; Kumar, K. Shiva
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2010 , vol. 49, # 3 p. 390 - 393
反应条件
1: With hydrogenchloride in water T=20°C; pH=1 - 3; 0.5 h; 2: in water chemoselective reaction;
参考文献
Li, Ping; Teng, Bo-Tao; Jin, Fa-Gen; Li, Xin-Sheng; Zhu, Wei-Dong; Xie, Jian-Wu
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 2 p. 244 - 247
反应条件
sodium lauryl sulfate in water T=25 - 30°C; 0.283333 h;
参考文献
Sharma, Saikat Das; Gogoi, Pranjal; Konwar, Dilip
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2007 , vol. 46, # 10 p. 1672 - 1678
反应条件
sodium lauryl sulfate in water T=25 - 30°C; 0.216667 h;
参考文献
Sharma, Saikat Das; Gogoi, Pranjal; Konwar, Dilip
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2007 , vol. 46, # 10 p. 1672 - 1678
反应条件
sodium lauryl sulfate in water T=25 - 30°C; 0.25 h;
参考文献
Sharma, Saikat Das; Gogoi, Pranjal; Konwar, Dilip
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2007 , vol. 46, # 10 p. 1672 - 1678
反应条件
Amberlite IRA-400(OH-) in ethanol 4 h; Heating;
参考文献
Konwar, Dilip; Dutta, Dilip Kumar; Goswami, Birendra Nath
Journal of Chemical Research - Part S, 1998 , # 6 p. 342 - 343
反应条件
1: hydroxylamine hydrochloride; sodium hydroxide / water / 4 h / 20 °C / pH 11 2: hydrogenchloride / water / 0.5 h / 20 °C / pH 1 - 3 View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 2 p. 244 - 247
反应条件
piperidine in ethanol
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 37, # 5 p. 484 - 490
反应条件
1: 2-cyano-3-phenyl-propionic acid amide With potassium hydride in acetonitrile T=20°C; 0.333333 h; Inert atmosphereGlovebox; 2: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium in acetonitrile T=24.84°C; Inert atmosphereGlovebox; Thermodynamic data;
参考文献
Journal of Organic Chemistry, , vol. 78, # 14 p. 7154 - 7168
反应条件
analog verlaeuft die Reaktion mit Furfurol;
参考文献
Chemische Berichte, , vol. 28, p. 2255