CH3CH2CH2CH2Li in tetrahydrofuran (N2); dissolving butyllithium and anthracene deriv. in THF, stirring at -78°C for 2 h, addn. of dioxaborolane deriv., stirring at -78°C for 5 h; addn, to water, extn. (ether), drying over MgSO4, concg., chromy. (silica gel, ethyl acetate/petroleum ether (1:40)), elem. anal.;

triethylamine; tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C; 12 h;

[(Pd(.mu.-Cl)(.kappa.(2)-P,C-P(OC6H2-2,4-tBu2)(OC6H3-2,4-tBu2)2))2]; C25H23OP; potassium acetate in N,N-dimethyl acetamide T=100°C; Miyaura borylation; 12 h; Inert atmosphere;

bis-triphenylphosphine-palladium(II) chloride; triethylamine in toluene Suzuki-Miyaura Coupling; 24 h; Inert atmosphereRefluxPhotolysis;

n-butyllithium in diethyl ether; hexane

copper(l) iodide; iron (III) acetylacetonate; N,N,N',N,-tetramethylethylenediamine; sodium hydride in tetrahydrofuran; mineral oil T=-10°C; Inert atmosphere;

potassium acetate; palladium diacetate in toluene T=60°C; 16 h; Inert atmosphere;

1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=30°C; 0.166667 h; Inert atmosphere; 2: 9-bromo-anthracene in ethylene glycol dimethyl ether T=30°C; 1 h;

Aliquatreg; 336; potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; toluene T=90°C; 7 h;