(3-羟基-5-甲氧基苯基)乙腈合成路线 （共 4 条）
反应条件
in 1-methyl-pyrrolidin-2-one
5 h;
参考文献
Weist, Stefan; Kittel, Claudia; Bischoff, Daniel; Bister, Bojan; Pfeifer, Volker; Nicholson, Graeme J.; Wohlleben, Wolfgang; Suessmuth, Roderich D.
Journal of the American Chemical Society, 2004 , vol. 126, # 19 p. 5942 - 5943
反应条件
1: 84 percent / triethylamine / tetrahydrofuran
2: 74 percent / BH3*THF / tetrahydrofuran / 12 h
3: 80 percent / PBr3 / tetrahydrofuran / 2 h
4: 56 percent / 1-methyl-pyrrolidin-2-one / 5 h
View Scheme
参考文献
Weist, Stefan; Kittel, Claudia; Bischoff, Daniel; Bister, Bojan; Pfeifer, Volker; Nicholson, Graeme J.; Wohlleben, Wolfgang; Suessmuth, Roderich D.
Journal of the American Chemical Society, 2004 , vol. 126, # 19 p. 5942 - 5943
反应条件
1: 74 percent / BH3*THF / tetrahydrofuran / 12 h
2: 80 percent / PBr3 / tetrahydrofuran / 2 h
3: 56 percent / 1-methyl-pyrrolidin-2-one / 5 h
View Scheme
参考文献
Weist, Stefan; Kittel, Claudia; Bischoff, Daniel; Bister, Bojan; Pfeifer, Volker; Nicholson, Graeme J.; Wohlleben, Wolfgang; Suessmuth, Roderich D.
Journal of the American Chemical Society, 2004 , vol. 126, # 19 p. 5942 - 5943
反应条件
1: 80 percent / PBr3 / tetrahydrofuran / 2 h
2: 56 percent / 1-methyl-pyrrolidin-2-one / 5 h
View Scheme
参考文献
Weist, Stefan; Kittel, Claudia; Bischoff, Daniel; Bister, Bojan; Pfeifer, Volker; Nicholson, Graeme J.; Wohlleben, Wolfgang; Suessmuth, Roderich D.
Journal of the American Chemical Society, 2004 , vol. 126, # 19 p. 5942 - 5943
