反应条件
1: 83 percent / Bu3SnH, azobis(isobutyronitrile) / benzene / Heating; other reagent: LiAlH4
2: 80 percent / CuSO4, p-TsOH / 4 h / 25 °C
3: 1.) MeLi, 2.) HMPA / 1.) hexane, 0 -> 25 deg C, 2 h, 2.) hexane, 25 deg C, 18 h
4: 19 mg / hydrogen, p-TsOH / Pd/C / methanol / 10 h / 25 °C
View Scheme
参考文献
Chen, Same-Ting; Fang, Jim-Min
Journal of Organic Chemistry, 1997 , vol. 62, # 13 p. 4349 - 4357
