2,2-二甲基-5-(2-哌啶基亚基)-1,3-二恶烷-4,6-二酮合成路线 （共 5 条）
参考文献
Celerier, J. P.; Maitte, P.
Tetrahedron Letters, 1981 , vol. 22, p. 963 - 964
反应条件
piperidine; triethylamine in benzene
24 h; Heating;
参考文献
Cheng; Zhao; Wang; Huang
Synthetic Communications, 1995 , vol. 25, # 9 p. 1339 - 1351
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene) in benzene
T=120°C; 26 h; Sealed tubeInert atmosphere;
参考文献
Koduri, Naga Durgarao; Scott, Halee; Hileman, Bethany; Cox, Justin D.; Coffin, Michael; Glicksberg, Lindsay; Hussaini, Syed R.
Organic Letters, 2012 , vol. 14, # 2 p. 440 - 443
反应条件
1: Lawesson's reagent / dichloromethane / 2 h / 20 °C
2: RuCl2(tricyclohexylphosphine)2(benzylidene) / benzene / 26 h / 120 °C / Sealed tube; Inert atmosphere
View Scheme
参考文献
Koduri, Naga Durgarao; Scott, Halee; Hileman, Bethany; Cox, Justin D.; Coffin, Michael; Glicksberg, Lindsay; Hussaini, Syed R.
Organic Letters, 2012 , vol. 14, # 2 p. 440 - 443
反应条件
1: 4-toluenesulfonyl azide; triethylamine / acetonitrile / 6.5 h / 0 - 20 °C
2: RuCl2(tricyclohexylphosphine)2(benzylidene) / benzene / 26 h / 120 °C / Sealed tube; Inert atmosphere
View Scheme
参考文献
Koduri, Naga Durgarao; Scott, Halee; Hileman, Bethany; Cox, Justin D.; Coffin, Michael; Glicksberg, Lindsay; Hussaini, Syed R.
Organic Letters, 2012 , vol. 14, # 2 p. 440 - 443
