N1-异丙基-1,2-苯二胺合成路线 (共 9 条)
参考文献
Malavaud, Christian; N'Gando M'Pondo, Teophile; Lopez, Lucien; Barrans, Jean; Legros, Jean-Pierre
Canadian Journal of Chemistry, 1984 , vol. 62, p. 43 - 50
反应条件
in tetrahydrofuran 20 h; Ambient temperature;
参考文献
Tapia, Ines; Alonso-Cires, Luisa; Lopez-Tudanca, Pedro Luis; Mosquera, Ramon; Labeaga, Luis; Innerarity, Ana; Orjales, Aurelio
Journal of Medicinal Chemistry, 1999 , vol. 42, # 15 p. 2870 - 2880
反应条件
palladium on activated charcoal; hydrogen in ethanol
T=20°C; 48 h; Inert atmosphere;
参考文献
Chen, Wen-Ching; Hsu, Yu-Chen; Lee, Ching-Yu; Yap, Glenn P. A.; Ong, Tiow-Gan
Organometallics, 2013 , vol. 32, # 8 p. 2435 - 2442
反应条件
1: 92 percent / BH3*SMe2 / CH2Cl2; acetic acid / 24 h / 20 °C
2: 98 percent / H2 / Pd/C / ethanol / 12 h / 20 °C
View Scheme
参考文献
Figge, Axel; Altenbach, Hans J.; Brauer, David J.; Tielmann, Patrick
Tetrahedron Asymmetry, 2002 , vol. 13, # 2 p. 137 - 144
反应条件
1: 36 h / 150 °C
2: H2 / 5percent Pd/C / ethanol / 4 h / Ambient temperature
View Scheme
参考文献
Jacobsen, E. Jon; Stelzer, Lindsay S.; Belonga, Kenneth L.; Carter, Donald B.; Im, Wha Bin; Sethy, Vimala H.; Tang, Andrew H.; Von Voigtlander, Philip F.; Petke, James D.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 19 p. 3820 - 3836
反应条件
1: 89 percent / 6 h / 150 °C
2: 84 percent / reduced iron, ammonium chloride / propan-1-ol / Heating
View Scheme
参考文献
Hawkins, David; Lindley, John M.; McRobbie, Ian M.; Meth-Cohn, Otto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2387 - 2391
反应条件
sodium hydroxide; borane
1.) THF, RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Morales, Hilda R.; Perez-Juarez, Martin; Cuellar, Laura; Mendoza, Lourdes; Fernandez, Hector; Contreras, Rosalinda
Synthetic Communications, 1984 , vol. 14, # 13 p. 1213 - 1220
参考文献
Major
Journal of the American Chemical Society, 1931 , vol. 53, p. 4373,4377
反应条件
dimethyl amine; tris-(dimethylamino)-phosphine
参考文献
Malavaud,C. et al.
Tetrahedron Letters, 1979 , p. 447 - 450