1,1,2-三甲基环己烷合成路线 （共 12 条）
反应条件
triethyl aluminum sesquichloride in dichloromethane
T=-18 - 20°C; 3 h;
参考文献
Biermann, Ursula; Metzger, Juergen O.
Journal of the American Chemical Society, 2004 , vol. 126, # 33 p. 10319 - 10330
反应条件
bis(cyclopentadienyl)titanium dichloride; triethylaluminum in hexane
T=20 - 25°C; 8 h; Title compound not separated from byproducts;
参考文献
Ramazanov; Sharipova; Dzhemilev
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 12 p. 1858 - 1860
反应条件
hydrogen; nickel in methanol
参考文献
Alder,K. et al.
Chemische Berichte, 1961 , vol. 94, p. 456 - 467
反应条件
hydrogen; nickel in methanol
参考文献
Alder,K. et al.
Chemische Berichte, 1961 , vol. 94, p. 456 - 467
反应条件
2: I2 / (heating)
3: H2 / Raney-Ni / methanol
View Scheme
参考文献
Alder,K. et al.
Chemische Berichte, 1961 , vol. 94, p. 456 - 467
反应条件
1: I2 / (heating)
2: H2 / Raney-Ni / methanol
View Scheme
参考文献
Alder,K. et al.
Chemische Berichte, 1961 , vol. 94, p. 456 - 467
反应条件
2: (i) Et2O, (ii) I2, (heating)
3: 380 °C / 12 Torr
4: H2 / Raney-Ni / methanol
View Scheme
参考文献
Alder,K. et al.
Chemische Berichte, 1961 , vol. 94, p. 456 - 467
反应条件
1: (i) Et2O, (ii) I2, (heating)
2: 380 °C / 12 Torr
3: H2 / Raney-Ni / methanol
View Scheme
参考文献
Alder,K. et al.
Chemische Berichte, 1961 , vol. 94, p. 456 - 467
反应条件
hydrogen; ozone; platinum(IV) oxide
1.) MeOAc, -72 deg C, 1 h, 2.) 160 deg C, 3 min; Multistep reaction;
参考文献
Whitfield, Frank B.; Sugowdz, Galina
Australian Journal of Chemistry, 1982 , vol. 35, # 3 p. 591 - 600
反应条件
aluminum tri-bromide; carbon tetrabromide in various solvent(s)
T=20°C; 0.5 h; Product distribution; Further Variations:Reagents;
参考文献
Akhrem; Churilova; Vitt
Russian Chemical Bulletin, 2001 , vol. 50, # 1 p. 81 - 87
