反应条件
1: 39 percent / BuLi 2: LiAlH4 / diethyl ether / 1) 0 deg C, 30 min, 2) r.t., 90 min 3: trifluoroacetic acid / 48 h / Heating 4: 73 percent / aq. sodium bicarbonate / CH2Cl2 / 22 h / Ambient temperature 5: 1) SOCl2, 2) potassium tert-butoxide / 1) THF, r.t, 17 h, 2) THF, 0 deg C, 0.5 h View Scheme
参考文献
Groundwater, Paul W.; Sharp, John T.
Tetrahedron, 1992 , vol. 48, # 37 p. 7951 - 7964